Technology Process of 2-phenyl(N,N,O)azoxy-6-methyldipyridi<1,2-a:3',2'-d>imidazole
There total 3 articles about 2-phenyl(N,N,O)azoxy-6-methyldipyridi<1,2-a:3',2'-d>imidazole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 73 percent / (CF3CO)2O, H2O2, Mo(CO)6 / trifluoroacetic acid; CH2Cl2 / 0 deg C -> room temperature
2: Al-Hg, H2O / tetrahydrofuran
3: 74 percent / acetic acid / 2 h / Ambient temperature
With
hexacarbonyl molybdenum; aluminium amalgam; water; dihydrogen peroxide; trifluoroacetic anhydride;
In
tetrahydrofuran; dichloromethane; acetic acid; trifluoroacetic acid;
DOI:10.1021/ja00390a040
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Al-Hg, H2O / tetrahydrofuran
2: 74 percent / acetic acid / 2 h / Ambient temperature
With
aluminium amalgam; water;
In
tetrahydrofuran; acetic acid;
DOI:10.1021/ja00390a040