N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

Base Information

• Chemical Name: N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine
• CAS No.: 442851-96-9
• Molecular Formula: C₂₇H₄₁NO₆
• Molecular Weight: 475.626

Synonyms:N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

Chemical Property of N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

There total 7 articles about N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C34H45NO6 (1243260-37-8) → N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine (442851-96-9)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; at 0 ℃; for 0.166667h;

Reference yield:

((3aS,4R,9aR,9bS)-2,8-Diphenyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-octyl-carbamic acid tert-butyl ester (442852-09-7) → N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine (442851-96-9)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; at 0 ℃; for 0.166667h;

DOI:10.1016/S0968-0896(02)00005-6

Reference yield:

benzaldehyde dimethyl acetal (1125-88-8) + N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine (442852-08-6) → N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine (442851-96-9) + ((3aS,4R,9aR,9bS)-2,8-Diphenyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-octyl-carbamic acid tert-butyl ester (442852-09-7)

Guidance literature:

With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 45 ℃; for 5.5h;

DOI:10.1016/S0968-0896(02)00005-6

upstream raw materials:

benzaldehyde dimethyl acetal

N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

((3aS,4R,9aR,9bS)-2,8-Diphenyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-octyl-carbamic acid tert-butyl ester

di-tert-butyl dicarbonate

Downstream raw materials:

N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

(1R,2S,3S,4S)-5-hydroxymethyl-1-octylamino-2,3,4-trihydroxycyclohex-5-ene

N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-6-O-tert-butyldimethylsilyl-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

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