C₆₅H₁₁₀O₁₀Si₄

Base Information

Chemical Name:C₆₅H₁₁₀O₁₀Si₄
CAS No.:200186-42-1
Molecular Formula:C₆₅H₁₁₀O₁₀Si₄
Molecular Weight:1163.92
Hs Code.:

C<sub>65</sub>H<sub>110</sub>O<sub>10</sub>Si<sub>4</sub>

Synonyms:C₆₅H₁₁₀O₁₀Si₄

Suppliers and Price of C₆₅H₁₁₀O₁₀Si₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₅H₁₁₀O₁₀Si₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₅H₁₁₀O₁₀Si₄

There total 20 articles about C₆₅H₁₁₀O₁₀Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 200186-49-8
C₄₉H₉₂O₁₀Si₃

: 200186-42-1
C₆₅H₁₁₀O₁₀Si₄

Guidance literature:: With dmap; In dichloromethane;
DOI:10.1016/S0040-4039(97)10499-3

Reference yield:

: 78999-24-3
5-benzyloxy-1-pentanal

: 200186-42-1
C₆₅H₁₁₀O₁₀Si₄

Guidance literature:: Multi-step reaction with 14 steps

1: 2.) BF₃*OEt₂; 2.) NaOH, H₂O₂ / 1.) -78 deg C

2: 89 percent / NaHMDS / tetrahydrofuran / 0 °C

3: IBr / toluene / -78 °C

4: K₂CO₃ / H₂O

5: 80 percent / n-BuLi, HMPA / tetrahydrofuran / -50 °C

6: 92 percent / PPTs / CH₂Cl₂

7: n-BuLi, HMPA / diethyl ether / -50 °C

8: 98 percent / 2,6-lutidine / CH₂Cl₂

9: 88 percent / TFA / CH₂Cl₂; H₂O / -10 °C

10: Hg(ClO₄)2, 2,6-lutidine / tetrahydrofuran / 0 °C

11: pyr

12: 56 percent / TMEDA / hexamethylphosphoric acid triamide / 80 °C

13: 78 percent / H₂, CaCO₃ / Pd/C / ethanol; ethyl acetate

14: 98 percent / DMAP / CH₂Cl₂

With pyridine; 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; sodium hydroxide; n-butyllithium; mercury(II) perchlorate; N,N,N,N,-tetramethylethylenediamine; boron trifluoride diethyl etherate; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; iodine(I) bromide; potassium carbonate; trifluoroacetic acid; calcium carbonate; palladium on activated charcoal; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; ethanol; dichloromethane; water; ethyl acetate; toluene;
DOI:10.1016/S0040-4039(97)10499-3

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 200186-42-1
C₆₅H₁₁₀O₁₀Si₄

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / TMEDA / hexamethylphosphoric acid triamide / 80 °C

2: 78 percent / H₂, CaCO₃ / Pd/C / ethanol; ethyl acetate

3: 98 percent / DMAP / CH₂Cl₂

With dmap; N,N,N,N,-tetramethylethylenediamine; hydrogen; calcium carbonate; palladium on activated charcoal; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4039(97)10499-3