3-hydroxy-2',3',4',5',6'-pentadeuteroflavone

Base Information

Chemical Name:3-hydroxy-2',3',4',5',6'-pentadeuteroflavone
CAS No.:104197-23-1
Molecular Formula:C₁₅H₁₀O₃
Molecular Weight:243.203
Hs Code.:

Synonyms:3-hydroxy-2',3',4',5',6'-pentadeuteroflavone

Suppliers and Price of 3-hydroxy-2',3',4',5',6'-pentadeuteroflavone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-hydroxy-2',3',4',5',6'-pentadeuteroflavone

Chemical Property:

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Technology Process of 3-hydroxy-2',3',4',5',6'-pentadeuteroflavone

There total 6 articles about 3-hydroxy-2',3',4',5',6'-pentadeuteroflavone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: C₁₅H₇⁽²⁾H₅O₂

: 104197-23-1
3-hydroxy-2',3',4',5',6'-pentadeuteroflavone

Guidance literature:: With dihydrogen peroxide; sodium hydroxide; In ethanol; water; at 20 ℃; for 12h;
DOI:10.1002/anie.201710049

Reference yield:

: 14132-51-5
2,3,4,5,6-pentadeuteriobenzaldehyde

: 104197-23-1
3-hydroxy-2',3',4',5',6'-pentadeuteroflavone

Guidance literature:: Multi-step reaction with 2 steps

1: alkaline

2: H₂O₂

With Alkaline; dihydrogen peroxide;
DOI:10.1002/oms.1210210305

Reference yield:

: 7379-67-1
d₅-iodobenzene

: 104197-23-1
3-hydroxy-2',3',4',5',6'-pentadeuteroflavone

Guidance literature:: Multi-step reaction with 3 steps

1: tricyclohexylphosphine; palladium diacetate; acetic anhydride; triethylamine / N,N-dimethyl-formamide / 7 h / 85 °C / Inert atmosphere

2: sodium hydroxide / ethanol; water / 12 h / 20 °C

3: sodium hydroxide; dihydrogen peroxide / ethanol; water / 12 h / 20 °C

With dihydrogen peroxide; palladium diacetate; acetic anhydride; triethylamine; sodium hydroxide; tricyclohexylphosphine; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201710049