Spiro[2,5-cyclohexadiene-1,3-[3H]indol]-2(1H)-one, 1-methyl- (9CI)

Base Information

Chemical Name:Spiro[2,5-cyclohexadiene-1,3-[3H]indol]-2(1H)-one, 1-methyl- (9CI)
CAS No.:797762-31-3
Molecular Formula:C14H13 N O
Molecular Weight:211.25912
Hs Code.:
Mol file:797762-31-3.mol

Synonyms:Spiro[2,5-cyclohexadiene-1,3-[3H]indol]-2(1H)-one, 1-methyl- (9CI)

Suppliers and Price of Spiro[2,5-cyclohexadiene-1,3-[3H]indol]-2(1H)-one, 1-methyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Spiro[2,5-cyclohexadiene-1,3-[3H]indol]-2(1H)-one, 1-methyl- (9CI)

Chemical Property:

PSA：20.31000
LogP:2.48190

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Spiro[2,5-cyclohexadiene-1,3-[3H]indol]-2(1H)-one, 1-methyl- (9CI)

There total 5 articles about Spiro[2,5-cyclohexadiene-1,3-[3H]indol]-2(1H)-one, 1-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 138883-34-8
N-(2-iodophenyl)-N-methylbenzamide

: 797762-31-3
1'-methylspiro[cyclohexane-1,3'-indoline]-2,5-dien-2'-one

Guidance literature:: With 1,3-dicyano-5-fluoro-2,4,6-tris(diphenylamino)benzene; water; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 23 ℃; for 16h; regioselective reaction; Inert atmosphere; Sealed tube; Irradiation; Green chemistry;
DOI:10.1021/jacs.0c03926

Reference yield: 39.0%

: 138883-34-8
N-(2-iodophenyl)-N-methylbenzamide

: 797762-31-3
1'-methylspiro[cyclohexane-1,3'-indoline]-2,5-dien-2'-one

: 797762-32-4
5-methyl-6a,10a-dihydrophenanthridin-6(5H)-one

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; isopropyl alcohol; In tetrahydrofuran; at 0 ℃; Further Variations:; Temperatures; Product distribution;
DOI:10.1039/b410457a

Reference yield:

: C₁₅H₁₂F₃NO₄S

: 797762-31-3
1'-methylspiro[cyclohexane-1,3'-indoline]-2,5-dien-2'-one

Guidance literature:: With formic acid; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 60 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol8016885