N-(2-Iodophenyl)benzamide

Base Information

• Chemical Name: N-(2-Iodophenyl)benzamide
• CAS No.: 15310-02-8
• Molecular Formula: C13H10 I N O
• Molecular Weight: 323.133
• NSC Number: 142518
• DSSTox Substance ID: DTXSID20934676
• Nikkaji Number: J1.944.880K
• Wikidata: Q82910617
• Mol file: 15310-02-8.mol

Synonyms:N-(2-Iodophenyl)benzamide;15310-02-8;NSC142518;N-(2-Iodophenyl)benzamide #;SCHEMBL6288808;Benzamide, N-(2'-iodophenyl)-;DTXSID20934676;HMS1759L12;AKOS001061969;NSC-142518;N-(2-Iodophenyl)benzenecarboximidic acid;10.14272/JNLAWMGPPJLSMA-UHFFFAOYSA-N;10.14272/JNLAWMGPPJLSMA-UHFFFAOYSA-N.1;AG-777/06841026;doi:10.14272/JNLAWMGPPJLSMA-UHFFFAOYSA-N;doi:10.14272/JNLAWMGPPJLSMA-UHFFFAOYSA-N.1;Z28163914

Chemical Property of N-(2-Iodophenyl)benzamide

Chemical Property:

• Vapor Pressure: 0.0007mmHg at 25°C
• Boiling Point: 308°Cat760mmHg
• Flash Point: 140.1°C
• Density: 1.697g/cm³
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 322.98071
• Heavy Atom Count: 16
• Complexity: 238

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)NC2=CC=CC=C2I

Technology Process of N-(2-Iodophenyl)benzamide

There total 8 articles about N-(2-Iodophenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-iodophenylamine (615-43-0) + benzoyl chloride (98-88-4) → o-iodobenzanilide (15310-02-8)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1021/jo051927q DOI:10.1016/j.tet.2007.08.013

Reference yield: 93.0%

benzoyl cyanide (613-90-1) + 2-iodophenylamine (615-43-0) → o-iodobenzanilide (15310-02-8)

Guidance literature:

In dimethyl sulfoxide; at 130 ℃; for 10h;

DOI:10.1021/acs.joc.9b03500

Reference yield: 81.0%

→ o-iodobenzanilide (15310-02-8)

Guidance literature:

With ammonium peroxydisulfate; tetrabutylammomium bromide; potassium hydroxide; In water; at 20 ℃; for 3h; Irradiation;

upstream raw materials:

2-iodophenylamine

benzoyl chloride

iodobenzene

carbon monoxide

Downstream raw materials:

N-(2-iodophenyl)-N-methylbenzamide

2-(2-Iodophenyl)-N-methoxymethylbenzamide

N-(but-3-en-1-yl)-N-(2-iodophenyl)benzamide

N-(2-iodophenyl)-N-(pent-4-en-1-yl)benzamide