Benzeneacetic acid, alpha-(hydroxymethyl)-2,5-dimethyl-, ethyl ester (9CI)

Base Information

Chemical Name:Benzeneacetic acid, alpha-(hydroxymethyl)-2,5-dimethyl-, ethyl ester (9CI)
CAS No.:797756-90-2
Molecular Formula:C13H18 O3
Molecular Weight:222.28022
Hs Code.:
Mol file:797756-90-2.mol

Synonyms:Benzeneacetic acid, alpha-(hydroxymethyl)-2,5-dimethyl-, ethyl ester (9CI)

Suppliers and Price of Benzeneacetic acid, alpha-(hydroxymethyl)-2,5-dimethyl-, ethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzeneacetic acid, alpha-(hydroxymethyl)-2,5-dimethyl-, ethyl ester (9CI)

Chemical Property:

PSA：46.53000
LogP:1.94240

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzeneacetic acid, alpha-(hydroxymethyl)-2,5-dimethyl-, ethyl ester (9CI)

There total 1 articles about Benzeneacetic acid, alpha-(hydroxymethyl)-2,5-dimethyl-, ethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 795274-98-5,797756-82-2
3-hydroxy-2-(2,5-dimethylphenyl)acrylic acid ethyl ester

: 797756-90-2,797756-95-7
3-hydroxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 8h;
DOI:10.1016/j.tetasy.2004.08.013

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 797756-90-2,797756-95-7
3-hydroxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

: 797756-95-7
(R)-(+)-3-hydroxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

: 797756-95-7
(S)-(-)-3-hydroxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

: (R)-(+)-3-acetoxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

: (S)-(-)-3-acetoxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

Guidance literature:: With Pseudomonas cepacia lipase; In toluene; at 20 ℃; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2004.08.013

Reference yield:

: 108-22-5
Isopropenyl acetate

: 797756-90-2,797756-95-7
3-hydroxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

: 797756-95-7
(R)-(+)-3-hydroxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

: 797756-95-7
(S)-(-)-3-hydroxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

: (R)-(+)-3-acetoxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

: (S)-(-)-3-acetoxy-2-(2,5-dimethylphenyl)-propionic acid ethyl ester

Guidance literature:: With lipase PS on celite support; ruthenium; In toluene; at 40 - 45 ℃; for 24h; Title compound not separated from byproducts.;
DOI:10.1016/j.tetlet.2007.03.143