Benzeneacetic acid, alpha-(hydroxymethylene)-2,5-dimethyl-, ethyl ester (9CI)

Base Information

Chemical Name:Benzeneacetic acid, alpha-(hydroxymethylene)-2,5-dimethyl-, ethyl ester (9CI)
CAS No.:795274-98-5
Molecular Formula:C₁₃H₁₆O₃
Molecular Weight:220.268
Hs Code.:
Mol file:795274-98-5.mol

Synonyms:Benzeneacetic acid, alpha-(hydroxymethylene)-2,5-dimethyl-, ethyl ester (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzeneacetic acid, alpha-(hydroxymethylene)-2,5-dimethyl-, ethyl ester (9CI)

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Technology Process of Benzeneacetic acid, alpha-(hydroxymethylene)-2,5-dimethyl-, ethyl ester (9CI)

There total 1 articles about Benzeneacetic acid, alpha-(hydroxymethylene)-2,5-dimethyl-, ethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 623-73-4
diazoacetic acid ethyl ester

: 5779-94-2
2,5-dimethylbenzaldehyde

: 63131-32-8
3-oxo-3-(2,5-dimethylphenyl)propanoic acid ethyl ester

: 795274-98-5,797756-82-2
3-hydroxy-2-(2,5-dimethylphenyl)acrylic acid ethyl ester

Guidance literature:: With cyclopentadienyldicarbonyl(tetrahydrofuran)iron(II) tetrafluoroborate; In dichloromethane; at 0 ℃; for 24h;
DOI:10.1021/jo0489418