1-<4-acetoxy-2-bis(ethoxycarbonylmethyl)aminophenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Base Information

Chemical Name:1-<4-acetoxy-2-bis(ethoxycarbonylmethyl)aminophenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane
CAS No.:149746-72-5
Molecular Formula:C₃₃H₄₄N₂O₁₂
Molecular Weight:660.719
Hs Code.:

Synonyms:1-<4-acetoxy-2-bis(ethoxycarbonylmethyl)aminophenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

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Chemical Property of 1-<4-acetoxy-2-bis(ethoxycarbonylmethyl)aminophenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

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Technology Process of 1-<4-acetoxy-2-bis(ethoxycarbonylmethyl)aminophenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

There total 6 articles about 1-<4-acetoxy-2-bis(ethoxycarbonylmethyl)aminophenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 105-36-2
ethyl bromoacetate

: 149746-71-4
1-(4-acetoxy-2-aminophenoxy)-2-(2-amino-5-methylphenoxy)ethane

: 149746-72-5
1-<4-acetoxy-2-bis(ethoxycarbonylmethyl)aminophenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Guidance literature:: With N-ethyl-N,N-diisopropylamine; at 140 ℃;

Reference yield:

: 96315-07-0
1-bromo-2-(2'-nitro-5'-methylphenoxy)ethane

: 149746-72-5
1-<4-acetoxy-2-bis(ethoxycarbonylmethyl)aminophenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Guidance literature:: Multi-step reaction with 5 steps

1: 45 percent / sodium carbonate / dimethylformamide / Heating

2: 82.2 percent / pyridine / 1 h

3: 87 percent / acetic acid, acetic anhydride, nitric acid / 1 h

4: 98 percent / H₂ / 5percent Pd/C / ethanol / 0.5 h

5: 70 percent / diisopropylethylamine (DIPEA) / 140 °C

With pyridine; hydrogen; nitric acid; acetic anhydride; sodium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 149746-72-5
1-<4-acetoxy-2-bis(ethoxycarbonylmethyl)aminophenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Guidance literature:: Multi-step reaction with 5 steps

1: 45 percent / sodium carbonate / dimethylformamide / Heating

2: 82.2 percent / pyridine / 1 h

3: 87 percent / acetic acid, acetic anhydride, nitric acid / 1 h

4: 98 percent / H₂ / 5percent Pd/C / ethanol / 0.5 h

5: 70 percent / diisopropylethylamine (DIPEA) / 140 °C

With pyridine; hydrogen; nitric acid; acetic anhydride; sodium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;