tert-butyl 2-[{[(tert-butyl)oxycarbonyl]methyl}(2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl)amino]acetate

Base Information

Chemical Name:tert-butyl 2-[{[(tert-butyl)oxycarbonyl]methyl}(2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl)amino]acetate
CAS No.:932711-48-3
Molecular Formula:C₂₄H₃₈INO₇
Molecular Weight:579.473
Hs Code.:

Synonyms:tert-butyl 2-[{[(tert-butyl)oxycarbonyl]methyl}(2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl)amino]acetate

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Chemical Property of tert-butyl 2-[{[(tert-butyl)oxycarbonyl]methyl}(2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl)amino]acetate

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Technology Process of tert-butyl 2-[{[(tert-butyl)oxycarbonyl]methyl}(2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl)amino]acetate

There total 4 articles about tert-butyl 2-[{[(tert-butyl)oxycarbonyl]methyl}(2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl)amino]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 932711-47-2
2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl 4-methylbenzenesulfonate

: 85916-13-8
tert-butyl iminodiacetate

: 932711-48-3
tert-butyl 2-[{[(tert-butyl)oxycarbonyl]methyl}(2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl)amino]acetate

Guidance literature:: In N,N-dimethyl-formamide; at 50 ℃; for 72h;
DOI:10.1021/jm061289j

Reference yield: 51.0%

: 932711-47-2
2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl 4-methylbenzenesulfonate

: 534-17-8
caesium carbonate

: 85916-13-8
tert-butyl iminodiacetate

: 932711-48-3
tert-butyl 2-[{[(tert-butyl)oxycarbonyl]methyl}(2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl)amino]acetate

: tert-butyl 2-[N-{[(tert-butyl)oxycarbonyl]methyl}(2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethoxy)carbonylamino]acetate

Guidance literature:: In N,N-dimethyl-formamide; at 70 ℃; for 720h;
DOI:10.1021/jm061289j

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 932711-48-3
tert-butyl 2-[{[(tert-butyl)oxycarbonyl]methyl}(2-{2-[2-(4-iodophenoxy)ethoxy]ethoxy}ethyl)amino]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / Cs₂CO₃ / dimethylformamide / 24 h / 50 °C

2: 70 percent / dimethylformamide / 72 h / 50 °C

With caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm061289j