N,N'-(4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)bis(4,1-phenylene))diacetamide

Base Information

Chemical Name:N,N'-(4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)bis(4,1-phenylene))diacetamide
CAS No.:1253850-55-3
Molecular Formula:C₂₉H₂₂Br₂N₂O₂
Molecular Weight:590.314
Hs Code.:

Synonyms:N,N'-(4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)bis(4,1-phenylene))diacetamide

Suppliers and Price of N,N'-(4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)bis(4,1-phenylene))diacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-(4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)bis(4,1-phenylene))diacetamide

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Technology Process of N,N'-(4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)bis(4,1-phenylene))diacetamide

There total 1 articles about N,N'-(4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)bis(4,1-phenylene))diacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 266315-56-4
4-(9-(4-aminophenyl)-2,7-dibromofluoren-9-yl)benzenamine

: 75-36-5
acetyl chloride

: 1253850-55-3
N,N'-(4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)bis(4,1-phenylene))diacetamide

Guidance literature:: In dichloromethane; at 20 ℃; for 4h;
DOI:10.1039/c0cc00136h

Reference yield: 54.0%

: 1253850-55-3
N,N'-(4,4'-(2,7-dibromo-9H-fluorene-9,9-diyl)bis(4,1-phenylene))diacetamide

: 371193-08-7
9,9-dihexylfluorene-2-boronic acid

: 1253850-47-3
TFAc

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 75 ℃; for 24h;
DOI:10.1039/c0cc00136h