allyl hydrogen 2-methyl-2-phenylmalonate

Base Information

Chemical Name:allyl hydrogen 2-methyl-2-phenylmalonate
CAS No.:930101-22-7
Molecular Formula:C₁₃H₁₄O₄
Molecular Weight:234.252
Hs Code.:

Synonyms:allyl hydrogen 2-methyl-2-phenylmalonate

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Chemical Property of allyl hydrogen 2-methyl-2-phenylmalonate

Chemical Property:

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Technology Process of allyl hydrogen 2-methyl-2-phenylmalonate

There total 3 articles about allyl hydrogen 2-methyl-2-phenylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930100-94-0
diallyl 2-methyl-2-phenylmalonate

: 930101-22-7
allyl hydrogen 2-methyl-2-phenylmalonate

: allyl hydrogen 2-methyl-2-phenylmalonate

Guidance literature:: With porcine liver esterase; sodium hydroxide; sodium dihydrogenphosphate; In water; at 20 ℃; for 72h; pH=7; Title compound not separated from byproducts;
DOI:10.1021/jo0621569

Reference yield:

: 930100-99-5
diallyl 2-phenylmalonate

: 930101-22-7
allyl hydrogen 2-methyl-2-phenylmalonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / cooling

1.2: 94 percent / tetrahydrofuran / 60 °C

2.1: porcine liver esterase; NaH₂PO₄; NaOH / H₂O / 72 h / 20 °C / pH 7

With porcine liver esterase; sodium hydroxide; sodium dihydrogenphosphate; sodium hydride; In tetrahydrofuran; water;
DOI:10.1021/jo0621569

Reference yield:

: 2613-89-0
phenylmalonic acid

: 930101-22-7
allyl hydrogen 2-methyl-2-phenylmalonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 94 percent / p-toluenesulfonic acid monohydrate / benzene / Heating

2.1: NaH / tetrahydrofuran / cooling

2.2: 94 percent / tetrahydrofuran / 60 °C

3.1: porcine liver esterase; NaH₂PO₄; NaOH / H₂O / 72 h / 20 °C / pH 7

With porcine liver esterase; sodium hydroxide; sodium dihydrogenphosphate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; water; benzene;
DOI:10.1021/jo0621569