5-chloromethyl-3-((R)-cyclohexyl-phenyl-trimethylsilanyloxy-methyl)-[1,2,4]oxadiazole

Base Information

Chemical Name:5-chloromethyl-3-((R)-cyclohexyl-phenyl-trimethylsilanyloxy-methyl)-[1,2,4]oxadiazole
CAS No.:1208428-34-5
Molecular Formula:C₁₉H₂₇ClN₂O₂Si
Molecular Weight:378.974
Hs Code.:

Synonyms:5-chloromethyl-3-((R)-cyclohexyl-phenyl-trimethylsilanyloxy-methyl)-[1,2,4]oxadiazole

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Chemical Property of 5-chloromethyl-3-((R)-cyclohexyl-phenyl-trimethylsilanyloxy-methyl)-[1,2,4]oxadiazole

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Technology Process of 5-chloromethyl-3-((R)-cyclohexyl-phenyl-trimethylsilanyloxy-methyl)-[1,2,4]oxadiazole

There total 1 articles about 5-chloromethyl-3-((R)-cyclohexyl-phenyl-trimethylsilanyloxy-methyl)-[1,2,4]oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207975-84-5
(R)-cyclohexyl-phenyl-trimethylsilanyloxy-acetaldehyde oxime

: 107-14-2
chloroacetonitrile

: 1208428-34-5
5-chloromethyl-3-((R)-cyclohexyl-phenyl-trimethylsilanyloxy-methyl)-[1,2,4]oxadiazole

Guidance literature:: (R)-cyclohexyl-phenyl-trimethylsilanyloxy-acetaldehyde oxime; With tert-butylhypochlorite; In dichloromethane; at -78 ℃;

With triethylamine; In dichloromethane; at -78 - 0 ℃;

chloroacetonitrile; In dichloromethane; toluene; at 0 - 20 ℃; Reflux;

Reference yield: 35.0%

: 1208428-34-5
5-chloromethyl-3-((R)-cyclohexyl-phenyl-trimethylsilanyloxy-methyl)-[1,2,4]oxadiazole

: 1049636-99-8
(R)-(5-chloromethyl-[1 ,2,4]oxadiazol-3-yl)-cyclohexyl-phenyl-methanol

Guidance literature:: 5-chloromethyl-3-((R)-cyclohexyl-phenyl-trimethylsilanyloxy-methyl)-[1,2,4]oxadiazole; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; Cooling with ice;

With water; In tetrahydrofuran; ethyl acetate;