phenyl 1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

Base Information

Chemical Name:phenyl 1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside
CAS No.:220587-60-0
Molecular Formula:C₂₃H₄₀O₅SeSi₂
Molecular Weight:531.699
Hs Code.:

Synonyms:phenyl 1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

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Technology Process of phenyl 1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

There total 5 articles about phenyl 1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 220588-06-7
phenyl 1-seleno-β-D-ribofuranoside

: 220587-60-0
phenyl 1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

Guidance literature:: In pyridine;
DOI:10.1021/jo981435w

Reference yield:

: 645-96-5
Benzeneselenol

: 220587-60-0
phenyl 1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: BF₃*Et₂O / CH₂Cl₂

2: Amberlite IRA-420 / methanol

3: pyridine

With Amberlite IRA-420; boron trifluoride diethyl etherate; In pyridine; methanol; dichloromethane; 1: Substitution / 2: Deacetylation / 3: cyclocondensation;
DOI:10.1016/S0040-4039(99)02071-7

Reference yield:

: 74458-63-2
phenyl 2,3,5-tri-O-acetyl-1-seleno-β-D-ribofuranoside

: 220587-60-0
phenyl 1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: Amberlite IRA-420 / methanol

2: pyridine

With Amberlite IRA-420; In pyridine; methanol; 1: Deacetylation / 2: cyclocondensation;
DOI:10.1016/S0040-4039(99)02071-7