phenyl 2-O-(diphenylhydrazono)acetyl-1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

Base Information

Chemical Name:phenyl 2-O-(diphenylhydrazono)acetyl-1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside
CAS No.:220587-61-1
Molecular Formula:C₃₇H₅₀N₂O₆SeSi₂
Molecular Weight:753.945
Hs Code.:

Synonyms:phenyl 2-O-(diphenylhydrazono)acetyl-1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

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Chemical Property of phenyl 2-O-(diphenylhydrazono)acetyl-1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

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Technology Process of phenyl 2-O-(diphenylhydrazono)acetyl-1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

There total 7 articles about phenyl 2-O-(diphenylhydrazono)acetyl-1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 728-15-4
(2,2-diphenylhydrazono)acetic acid

: 220587-60-0
phenyl 1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

: 220587-61-1
phenyl 2-O-(diphenylhydrazono)acetyl-1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 12h;
DOI:10.1021/jo981435w

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 220587-61-1
phenyl 2-O-(diphenylhydrazono)acetyl-1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine

2: 94 percent / DCC, DMAP / CH₂Cl₂ / 12 h

With dmap; dicyclohexyl-carbodiimide; In pyridine; dichloromethane;
DOI:10.1021/jo981435w

Reference yield:

: 530-47-2,29666-92-0
N,N-diphenylhydrazine hydrochloride

: 220587-61-1
phenyl 2-O-(diphenylhydrazono)acetyl-1-seleno-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / H₂O / 2 h

2: 94 percent / DCC, DMAP / CH₂Cl₂ / 12 h

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; water;
DOI:10.1021/jo981435w