1,2-bis(4-(2-methyl-1,3-dioxolan-2-yl)phenyl)ditellane

Base Information

Chemical Name:1,2-bis(4-(2-methyl-1,3-dioxolan-2-yl)phenyl)ditellane
CAS No.:84280-95-5
Molecular Formula:C₂₀H₂₂O₄Te₂
Molecular Weight:581.592
Hs Code.:

Synonyms:1,2-bis(4-(2-methyl-1,3-dioxolan-2-yl)phenyl)ditellane

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Chemical Property of 1,2-bis(4-(2-methyl-1,3-dioxolan-2-yl)phenyl)ditellane

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Technology Process of 1,2-bis(4-(2-methyl-1,3-dioxolan-2-yl)phenyl)ditellane

There total 4 articles about 1,2-bis(4-(2-methyl-1,3-dioxolan-2-yl)phenyl)ditellane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 4360-68-3
2-(4-bromophenyl)-2-methyl-1,3-dioxolane

: 84280-95-5
1,2-bis(4-(2-methyl-1,3-dioxolan-2-yl)phenyl)ditellane

Guidance literature:: 2-(4-bromophenyl)-2-methyl-1,3-dioxolane; With magnesium; In tetrahydrofuran; for 4h; Reflux;

With tellurium; at 20 ℃;
DOI:10.1016/j.jorganchem.2018.08.007

Reference yield:

: 99-90-1
para-bromoacetophenone

: 84280-95-5
1,2-bis(4-(2-methyl-1,3-dioxolan-2-yl)phenyl)ditellane

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / p-toluenesulfonic acid / benzene / 15 h / Heating

2: 1.) magnesium, iodine, 2.) tellurium / 1.) THF, reflux, 2.) reflux, 3 h

With tellurium; iodine; toluene-4-sulfonic acid; magnesium; In benzene;
DOI:10.1021/ja00342a040

Reference yield:

: 99-90-1
para-bromoacetophenone

: 84280-95-5
1,2-bis(4-(2-methyl-1,3-dioxolan-2-yl)phenyl)ditellane

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / toluene / 12 h / Reflux

2.1: magnesium / tetrahydrofuran / 4 h / Reflux

2.2: 20 °C

With toluene-4-sulfonic acid; magnesium; In tetrahydrofuran; toluene;
DOI:10.1016/j.jorganchem.2018.08.007