C₂₇H₂₇N₅O₅S

Base Information

Chemical Name:C₂₇H₂₇N₅O₅S
CAS No.:1620955-71-6
Molecular Formula:C₂₇H₂₇N₅O₅S
Molecular Weight:533.608
Hs Code.:

C<sub>27</sub>H<sub>27</sub>N<sub>5</sub>O<sub>5</sub>S

Synonyms:C₂₇H₂₇N₅O₅S

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Chemical Property of C₂₇H₂₇N₅O₅S

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Technology Process of C₂₇H₂₇N₅O₅S

There total 10 articles about C₂₇H₂₇N₅O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 870-46-2
t-butoxycarbonylhydrazine

: 1620955-70-5
C₂₂H₁₇N₃O₄S

: 1620955-71-6
C₂₇H₂₇N₅O₅S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 12h; Inert atmosphere;

Reference yield:

: 191338-94-0
ethyl {4-[(2,2-dimethylpropanoyl)amino]pyridin-3-yl}(oxo)acetate

: 1620955-71-6
C₂₇H₂₇N₅O₅S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide; water / ethanol / 2 h / Reflux

1.2: 16 h

2.1: methanol; diethyl ether / 1 h / 0 °C

3.1: potassium carbonate / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere

3.2: 8 h / Reflux

4.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 4 h / 0 - 20 °C

5.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1054478-77-1
2-(4-bromophenyl)-1,6-naphthyridine-4-carboxylic acid

: 1620955-71-6
C₂₇H₂₇N₅O₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol; diethyl ether / 1 h / 0 °C

2.1: potassium carbonate / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere

2.2: 8 h / Reflux

3.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 4 h / 0 - 20 °C

4.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; methanol; diethyl ether; water; N,N-dimethyl-formamide;