(+)-(1R,2R)-trans-1-(4-chloro-3-methoxyphenyl)-N-(2,2-dimethoxyethyl)-1,2,3,4-tetrahydro-N-methyl-2-naphthaleneamine oxalate salt

Base Information

Chemical Name:(+)-(1R,2R)-trans-1-(4-chloro-3-methoxyphenyl)-N-(2,2-dimethoxyethyl)-1,2,3,4-tetrahydro-N-methyl-2-naphthaleneamine oxalate salt
CAS No.:766537-21-7
Molecular Formula:C₂H₂O₄*C₂₂H₂₈ClNO₃
Molecular Weight:479.958
Hs Code.:

Synonyms:(+)-(1R,2R)-trans-1-(4-chloro-3-methoxyphenyl)-N-(2,2-dimethoxyethyl)-1,2,3,4-tetrahydro-N-methyl-2-naphthaleneamine oxalate salt

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Chemical Property of (+)-(1R,2R)-trans-1-(4-chloro-3-methoxyphenyl)-N-(2,2-dimethoxyethyl)-1,2,3,4-tetrahydro-N-methyl-2-naphthaleneamine oxalate salt

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Technology Process of (+)-(1R,2R)-trans-1-(4-chloro-3-methoxyphenyl)-N-(2,2-dimethoxyethyl)-1,2,3,4-tetrahydro-N-methyl-2-naphthaleneamine oxalate salt

There total 10 articles about (+)-(1R,2R)-trans-1-(4-chloro-3-methoxyphenyl)-N-(2,2-dimethoxyethyl)-1,2,3,4-tetrahydro-N-methyl-2-naphthaleneamine oxalate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: bromo-(4-chloro-3-methoxy-phenyl)magnesium

: Toluene-4-sulfonic acid (1R,2R)-1-[(2,2-dimethoxy-ethyl)-methyl-amino]-1,2,3,4-tetrahydro-naphthalen-2-yl ester

: 766537-21-7
(+)-(1R,2R)-trans-1-(4-chloro-3-methoxyphenyl)-N-(2,2-dimethoxyethyl)-1,2,3,4-tetrahydro-N-methyl-2-naphthaleneamine oxalate salt

Guidance literature:: copper(I) cyanide; In tetrahydrofuran; hexanes; diethylene glycol dimethyl ether; at -5 - 45 ℃; for 1 - 2h;

Reference yield:

: bromo-(4-chloro-3-methoxy-phenyl)magnesium

: Phosphoric acid (1R,2R)-1-[(2,2-dimethoxy-ethyl)-methyl-amino]-1,2,3,4-tetrahydro-naphthalen-2-yl ester diphenyl ester

: 766537-21-7
(+)-(1R,2R)-trans-1-(4-chloro-3-methoxyphenyl)-N-(2,2-dimethoxyethyl)-1,2,3,4-tetrahydro-N-methyl-2-naphthaleneamine oxalate salt

Guidance literature:: CuCl*2LiCl; In tetrahydrofuran; hexanes; diethylene glycol dimethyl ether; at 30 - 45 ℃; for 1 - 2h;

Reference yield:

: 144-62-7,97993-78-7
oxalic acid

: bromo-(4-chloro-3-methoxy-phenyl)magnesium

: Phosphoric acid (1R,2R)-1-[(2,2-dimethoxy-ethyl)-methyl-amino]-1,2,3,4-tetrahydro-naphthalen-2-yl ester diphenyl ester

: 766537-21-7
(+)-(1R,2R)-trans-1-(4-chloro-3-methoxyphenyl)-N-(2,2-dimethoxyethyl)-1,2,3,4-tetrahydro-N-methyl-2-naphthaleneamine oxalate salt

Guidance literature:: bromo-(4-chloro-3-methoxy-phenyl)magnesium; Phosphoric acid (1R,2R)-1-[(2,2-dimethoxy-ethyl)-methyl-amino]-1,2,3,4-tetrahydro-naphthalen-2-yl ester diphenyl ester; With copper(I) chloride bis(lithium chloride) complex; In tetrahydrofuran; at 25 - 45 ℃; for 2.15h; Inert atmosphere;

oxalic acid; In isopropyl alcohol; at 45 ℃; Inert atmosphere;
DOI:10.1021/op0402026