2'-bromo-2-phenylspiro[3,1-benzoxazine-4,1'-cyclopentane] hydrobromide

Base Information

Chemical Name:2'-bromo-2-phenylspiro[3,1-benzoxazine-4,1'-cyclopentane] hydrobromide
CAS No.:1333467-39-2
Molecular Formula:BrH*C₁₈H₁₆BrNO
Molecular Weight:423.147
Hs Code.:

Synonyms:2'-bromo-2-phenylspiro[3,1-benzoxazine-4,1'-cyclopentane] hydrobromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-bromo-2-phenylspiro[3,1-benzoxazine-4,1'-cyclopentane] hydrobromide

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Technology Process of 2'-bromo-2-phenylspiro[3,1-benzoxazine-4,1'-cyclopentane] hydrobromide

There total 3 articles about 2'-bromo-2-phenylspiro[3,1-benzoxazine-4,1'-cyclopentane] hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1254836-95-7
N-(2-cyclopent-1-en-1-ylphenyl)benzamide

: 1333467-39-2
2'-bromo-2-phenylspiro[3,1-benzoxazine-4,1'-cyclopentane] hydrobromide

Guidance literature:: With bromine; In tetrachloromethane; for 0.333333h;
DOI:10.1007/s10593-011-0764-6

Reference yield:

: 1254837-16-5
2-phenylspiro[3,1-benzoxazine-4,1'-cyclopentane]

: 1333467-39-2
2'-bromo-2-phenylspiro[3,1-benzoxazine-4,1'-cyclopentane] hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 1 h / 250 °C / Inert atmosphere

2: bromine / tetrachloromethane / 0.33 h

With bromine; In tetrachloromethane;
DOI:10.1007/s10593-011-0764-6

Reference yield:

: 98-88-4
benzoyl chloride

: 1333467-39-2
2'-bromo-2-phenylspiro[3,1-benzoxazine-4,1'-cyclopentane] hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dichloromethane / 24 h / 20 °C

2: bromine / tetrachloromethane / 0.33 h

With bromine; potassium carbonate; In tetrachloromethane; dichloromethane;
DOI:10.1007/s10593-011-0764-6