Technology Process of C29H28F3NO6
There total 4 articles about C29H28F3NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
magnesium iodide diethyletherate;
In
tetrahydrofuran; diethyl ether;
at 0 - 50 ℃;
for 5h;
DOI:10.1002/anie.201308016
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
1.2: 0.33 h / -78 °C
1.3: -78 - 20 °C
2.1: trimethylsilyl trifluoromethanesulfonate; calcium sulfate / 1,2-dichloro-ethane / 19 h / -30 - 30 °C / Inert atmosphere
3.1: magnesium iodide diethyletherate / diethyl ether; tetrahydrofuran / 5 h / 0 - 50 °C
With
calcium sulfate; magnesium iodide diethyletherate; trimethylsilyl trifluoromethanesulfonate; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1002/anie.201308016
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
1.2: 0.33 h / -78 °C
1.3: -78 - 20 °C
2.1: trimethylsilyl trifluoromethanesulfonate; calcium sulfate / 1,2-dichloro-ethane / 19 h / -30 - 30 °C / Inert atmosphere
3.1: magnesium iodide diethyletherate / diethyl ether; tetrahydrofuran / 5 h / 0 - 50 °C
With
calcium sulfate; magnesium iodide diethyletherate; trimethylsilyl trifluoromethanesulfonate; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1002/anie.201308016
