Technology Process of C17H15NO4
There total 2 articles about C17H15NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
phthalimide;
In
N,N-dimethyl-formamide;
at 90 ℃;
optical yield given as %ee;
Inert atmosphere;
DOI:10.1002/chem.201003320
- Guidance literature:
-
Multi-step reaction with 2 steps
1: osmium(VIII) oxide; potassium hexacyanoferrate(III); methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether / water; tert-butyl alcohol / 48 h / 0 °C / Inert atmosphere
2: phthalimide / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
With
osmium(VIII) oxide; phthalimide; methanesulfonamide; potassium hexacyanoferrate(III); sodium hydrogencarbonate; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether;
In
water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/chem.201003320
- Guidance literature:
-
With
1,4-diaza-bicyclo[2.2.2]octane; trifluoromethylsulfonic anhydride;
In
dichloromethane;
at -78 - 20 ℃;
Inert atmosphere;
DOI:10.1002/chem.201003320