2,5-Dimethyl-6-phenyl-cyclohex-3-enecarboxylic acid ((1S,2R)-2-hydroxy-1-methyl-2-phenyl-ethyl)-amide

Base Information

Chemical Name:2,5-Dimethyl-6-phenyl-cyclohex-3-enecarboxylic acid ((1S,2R)-2-hydroxy-1-methyl-2-phenyl-ethyl)-amide
CAS No.:130178-09-5
Molecular Formula:C₂₄H₂₉NO₂
Molecular Weight:363.5
Hs Code.:

Synonyms:2,5-Dimethyl-6-phenyl-cyclohex-3-enecarboxylic acid ((1S,2R)-2-hydroxy-1-methyl-2-phenyl-ethyl)-amide

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Chemical Property of 2,5-Dimethyl-6-phenyl-cyclohex-3-enecarboxylic acid ((1S,2R)-2-hydroxy-1-methyl-2-phenyl-ethyl)-amide

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Technology Process of 2,5-Dimethyl-6-phenyl-cyclohex-3-enecarboxylic acid ((1S,2R)-2-hydroxy-1-methyl-2-phenyl-ethyl)-amide

There total 3 articles about 2,5-Dimethyl-6-phenyl-cyclohex-3-enecarboxylic acid ((1S,2R)-2-hydroxy-1-methyl-2-phenyl-ethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 130178-08-4
(4S,5R)-3-(2,5-Dimethyl-6-phenyl-cyclohex-3-enecarbonyl)-4-methyl-5-phenyl-oxazolidin-2-one

: 130178-09-5
2,5-Dimethyl-6-phenyl-cyclohex-3-enecarboxylic acid ((1S,2R)-2-hydroxy-1-methyl-2-phenyl-ethyl)-amide

Guidance literature:: With lithium aluminium tetrahydride;
DOI:10.1016/0040-4039(90)80164-H

Reference yield:

: 5194-51-4
(2E,4E)-hexa-2,4-diene

: 130178-09-5
2,5-Dimethyl-6-phenyl-cyclohex-3-enecarboxylic acid ((1S,2R)-2-hydroxy-1-methyl-2-phenyl-ethyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 72 h / 180 °C

2: 81 percent / LiAlH₄

With lithium aluminium tetrahydride;
DOI:10.1016/0040-4039(90)80164-H

Reference yield:

: 130272-30-9
(E)-(4S,5R)-4-methyl-3-(3'-phenyl-2'-propenoyl)-5-phenyl-2-oxazolidinone

: 130178-09-5
2,5-Dimethyl-6-phenyl-cyclohex-3-enecarboxylic acid ((1S,2R)-2-hydroxy-1-methyl-2-phenyl-ethyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 72 h / 180 °C

2: 81 percent / LiAlH₄

With lithium aluminium tetrahydride;
DOI:10.1016/0040-4039(90)80164-H