C₄₁H₄₉N₇O₂

Base Information

Chemical Name:C₄₁H₄₉N₇O₂
CAS No.:1028256-98-5
Molecular Formula:C₄₁H₄₉N₇O₂
Molecular Weight:671.886
Hs Code.:

C<sub>41</sub>H<sub>49</sub>N<sub>7</sub>O<sub>2</sub>

Synonyms:C₄₁H₄₉N₇O₂

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Chemical Property of C₄₁H₄₉N₇O₂

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Technology Process of C₄₁H₄₉N₇O₂

There total 10 articles about C₄₁H₄₉N₇O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1466-67-7
1,3-dibenzylurea

: 1028256-98-5
C₄₁H₄₉N₇O₂

Guidance literature:: Multi-step reaction with 5 steps

1: 1) i-Pr₂NEt / 1) H₂O, 10 min, 2) EtOAc, reflux

2: 80 percent / LiBH₄ / tetrahydrofuran / Heating

3: i-Pr₂NEt / CH₂Cl₂ / 0.17 h / 0 °C

4: NaN₃ / dimethylformamide / 1.25 h / 80 °C

5: 1) PPh₃, molecular sieves 4 Angstroem / 1) THF, 23 deg C, 45 min, 2) THF, 30 min

With lithium borohydride; sodium azide; 4 A molecular sieve; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00049a036

Reference yield:

: 3173-56-6
benzyl isothiocyanate

: 1028256-98-5
C₄₁H₄₉N₇O₂

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / CH₂Cl₂ / 0.5 h / 5 °C

2: 1) i-Pr₂NEt / 1) H₂O, 10 min, 2) EtOAc, reflux

3: 80 percent / LiBH₄ / tetrahydrofuran / Heating

4: i-Pr₂NEt / CH₂Cl₂ / 0.17 h / 0 °C

5: NaN₃ / dimethylformamide / 1.25 h / 80 °C

6: 1) PPh₃, molecular sieves 4 Angstroem / 1) THF, 23 deg C, 45 min, 2) THF, 30 min

With lithium borohydride; sodium azide; 4 A molecular sieve; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00049a036

Reference yield:

: 100-46-9
benzylamine

: 1028256-98-5
C₄₁H₄₉N₇O₂

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / CH₂Cl₂ / 0.5 h / 5 °C

2: 1) i-Pr₂NEt / 1) H₂O, 10 min, 2) EtOAc, reflux

3: 80 percent / LiBH₄ / tetrahydrofuran / Heating

4: i-Pr₂NEt / CH₂Cl₂ / 0.17 h / 0 °C

5: NaN₃ / dimethylformamide / 1.25 h / 80 °C

6: 1) PPh₃, molecular sieves 4 Angstroem / 1) THF, 23 deg C, 45 min, 2) THF, 30 min

With lithium borohydride; sodium azide; 4 A molecular sieve; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00049a036