benzyl (R)-3-(tert-butyldimethylsiloxy)-2-(diphenylacetyloxy)propanoate

Base Information

Chemical Name:benzyl (R)-3-(tert-butyldimethylsiloxy)-2-(diphenylacetyloxy)propanoate
CAS No.:1208982-44-8
Molecular Formula:C₃₀H₃₆O₅Si
Molecular Weight:504.698
Hs Code.:

Synonyms:benzyl (R)-3-(tert-butyldimethylsiloxy)-2-(diphenylacetyloxy)propanoate

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Chemical Property of benzyl (R)-3-(tert-butyldimethylsiloxy)-2-(diphenylacetyloxy)propanoate

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Technology Process of benzyl (R)-3-(tert-butyldimethylsiloxy)-2-(diphenylacetyloxy)propanoate

There total 4 articles about benzyl (R)-3-(tert-butyldimethylsiloxy)-2-(diphenylacetyloxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1760-46-9
diphenylacetic anhydride

: 131711-06-3
benzyl 3-(tert-butyldimethylsiloxy)-2-hydroxypropanoate

: 1208982-44-8
benzyl (R)-3-(tert-butyldimethylsiloxy)-2-(diphenylacetyloxy)propanoate

: 310404-56-9
benzyl (S)-3-(tert-butyldimethylsilyloxy)-2-hydroxypropanoate

Guidance literature:: With (R)-(+)-2-phenyl-2,3-dihydrobenzo[d]imidazo[2,1-b]thiazole; 2,2-dimethylpropanoic anhydride; N-ethyl-N,N-diisopropylamine; In diethyl ether; at 20 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.08.018

Reference yield: 47.0%

: 117-34-0
2,2-diphenylacetic acid

: 131711-06-3
benzyl 3-(tert-butyldimethylsiloxy)-2-hydroxypropanoate

: benzyl (R)-3-(tert-butyldimethylsiloxy)-2-hydroxypropanoate

: 1208982-44-8
benzyl (R)-3-(tert-butyldimethylsiloxy)-2-(diphenylacetyloxy)propanoate

: 310404-56-9
benzyl (S)-3-(tert-butyldimethylsilyloxy)-2-hydroxypropanoate

Guidance literature:: With (R)-(+)-2-phenyl-2,3-dihydrobenzo[d]imidazo[2,1-b]thiazole; 2,2-dimethylpropanoic anhydride; N-ethyl-N,N-diisopropylamine; In diethyl ether; at 20 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Resolution of racemate;
DOI:10.1002/chem.200902257

Reference yield: 46.0%

: 1760-46-9
diphenylacetic anhydride

: 131711-06-3
benzyl 3-(tert-butyldimethylsiloxy)-2-hydroxypropanoate

: benzyl (R)-3-(tert-butyldimethylsiloxy)-2-hydroxypropanoate

: 1208982-44-8
benzyl (R)-3-(tert-butyldimethylsiloxy)-2-(diphenylacetyloxy)propanoate

: 310404-56-9
benzyl (S)-3-(tert-butyldimethylsilyloxy)-2-hydroxypropanoate

Guidance literature:: With (R)-(+)-2-phenyl-2,3-dihydrobenzo[d]imidazo[2,1-b]thiazole; N-ethyl-N,N-diisopropylamine; In diethyl ether; at 20 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.08.018