<α-(trimethylsilyl)benzyl>lithium N,N,N'N'-tetramethylethylenediamne complex

Base Information

• Chemical Name: <α-(trimethylsilyl)benzyl>lithium N,N,N'N'-tetramethylethylenediamne complex
• CAS No.: 105034-70-6
• Molecular Formula: C₆H₁₆N₂*C₁₀H₁₅Si*Li
• Molecular Weight: 286.462

Synonyms:<α-(trimethylsilyl)benzyl>lithium N,N,N'N'-tetramethylethylenediamne complex

Chemical Property of <α-(trimethylsilyl)benzyl>lithium N,N,N'N'-tetramethylethylenediamne complex

Chemical Property:

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Technology Process of <α-(trimethylsilyl)benzyl>lithium N,N,N'N'-tetramethylethylenediamne complex

There total 2 articles about <α-(trimethylsilyl)benzyl>lithium N,N,N'N'-tetramethylethylenediamne complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

N,N,N,N,-tetramethylethylenediamine (110-18-9) + benzyltrimethylsilane (770-09-2) → <α-(trimethylsilyl)benzyl>lithium N,N,N'N'-tetramethylethylenediamne complex (105034-70-6)

Guidance literature:

With n-butyllithium; In light petroleum; hexane; at 20 ℃; for 12h;

DOI:10.1016/j.jorganchem.2009.06.025

Reference yield:

benzyltrimethylsilane (770-09-2) → <α-(trimethylsilyl)benzyl>lithium N,N,N'N'-tetramethylethylenediamne complex (105034-70-6)

Guidance literature:

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at 0 ℃; for 5h;

Reference yield: 94.0%

<α-(trimethylsilyl)benzyl>lithium N,N,N'N'-tetramethylethylenediamne complex (105034-70-6) + benzonitrile (100-47-0) → K[CH(Ph)C(Ph)NSiMe3] (1192621-72-9)

Guidance literature:

<α-(trimethylsilyl)benzyl>lithium N,N,N'N'-tetramethylethylenediamne complex; benzonitrile; In light petroleum; at 20 ℃; for 4h;

With potassium tert-butylate; In light petroleum; at 20 ℃; for 4h;

DOI:10.1016/j.jorganchem.2009.06.025

upstream raw materials:

benzyltrimethylsilane

N,N,N,N,-tetramethylethylenediamine

Downstream raw materials:

Li((CH₃)2NCH₂CH₂N(CH₃)2)2⁽¹⁺⁾*Zn(CH(Si(CH₃)3)C₆H₅)3^(1-)=(Li(C₆H₁₆N₂)2)(Zn(C₁₀H₁₅Si)3)

K[CH(Ph)C(Ph)NSiMe₃]

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