N-(3-chloro-4-fluoro-phenyl)-N-(7-methoxy-6-nitro-quinazoline-4-yl)-acetamide

Base Information

• Chemical Name: N-(3-chloro-4-fluoro-phenyl)-N-(7-methoxy-6-nitro-quinazoline-4-yl)-acetamide
• CAS No.: 869199-61-1
• Molecular Formula: C₁₇H₁₂ClFN₄O₄
• Molecular Weight: 390.758

Synonyms:N-(3-chloro-4-fluoro-phenyl)-N-(7-methoxy-6-nitro-quinazoline-4-yl)-acetamide

Chemical Property of N-(3-chloro-4-fluoro-phenyl)-N-(7-methoxy-6-nitro-quinazoline-4-yl)-acetamide

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

N-(3-Chloro-4-fluorophenyl)-N-(7-methoxy-6-nitroquinazolin-4-yl)acetamide 97% ^*data from reagent suppliers

Safty Information:

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Technology Process of N-(3-chloro-4-fluoro-phenyl)-N-(7-methoxy-6-nitro-quinazoline-4-yl)-acetamide

There total 1 articles about N-(3-chloro-4-fluoro-phenyl)-N-(7-methoxy-6-nitro-quinazoline-4-yl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.4%

N-(3-chloro-4-fluorophenyl)-7-methoxy-6-nitroquinazolin- 4-amine (179552-74-0) + acetic anhydride (108-24-7) → N-(3-chloro-4-fluoro-phenyl)-N-(7-methoxy-6-nitro-quinazoline-4-yl)-acetamide (869199-61-1)

Guidance literature:

at 90 ℃; for 24h;

Reference yield: 94.49%

N-(3-chloro-4-fluoro-phenyl)-N-(7-methoxy-6-nitro-quinazoline-4-yl)-acetamide (869199-61-1) → N-(6-amino-7-methoxy-quinazolin-4-yl)-N-(3-chloro-4-fluoro-phenyl)-acetamide (869199-62-2)

Guidance literature:

With hydrogen; nickel; In tetrahydrofuran; at 60 ℃; for 38h; under 3102.97 Torr;

upstream raw materials:

N-(3-chloro-4-fluorophenyl)-7-methoxy-6-nitroquinazolin- 4-amine

acetic anhydride

Downstream raw materials:

N-(6-amino-7-methoxy-quinazolin-4-yl)-N-(3-chloro-4-fluoro-phenyl)-acetamide

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