2-(((trans)-4-(tert-butyl)cyclohexyl)oxy)-4-(trifluoromethyl)-1-naphthaldehyde

Base Information

Chemical Name:2-(((trans)-4-(tert-butyl)cyclohexyl)oxy)-4-(trifluoromethyl)-1-naphthaldehyde
CAS No.:1621065-12-0
Molecular Formula:C₂₂H₂₅F₃O₂
Molecular Weight:378.435
Hs Code.:

Synonyms:2-(((trans)-4-(tert-butyl)cyclohexyl)oxy)-4-(trifluoromethyl)-1-naphthaldehyde

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Chemical Property of 2-(((trans)-4-(tert-butyl)cyclohexyl)oxy)-4-(trifluoromethyl)-1-naphthaldehyde

Chemical Property:

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Technology Process of 2-(((trans)-4-(tert-butyl)cyclohexyl)oxy)-4-(trifluoromethyl)-1-naphthaldehyde

There total 5 articles about 2-(((trans)-4-(tert-butyl)cyclohexyl)oxy)-4-(trifluoromethyl)-1-naphthaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 680-15-9
2,2-difluoro-2-(fluorosulfonyl)acetate

: 1621064-75-2
2-(((trans)-4-(tert-butyl)cyclohexyl)oxy)-4-iodo-1-naphthaldehyde

: 1621065-12-0
2-(((trans)-4-(tert-butyl)cyclohexyl)oxy)-4-(trifluoromethyl)-1-naphthaldehyde

Guidance literature:: With copper(l) iodide; In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide; at 80 ℃; for 4h; Inert atmosphere;

Reference yield:

: 90800-21-8
4-iodonaphthalen-2-ol

: 1621065-12-0
2-(((trans)-4-(tert-butyl)cyclohexyl)oxy)-4-(trifluoromethyl)-1-naphthaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / tert-butyl alcohol; butanone / 4 h / 100 °C / Sealed tube

2.1: tin(IV) chloride / dichloromethane / 2 h / 0 - 20 °C

2.2: 2 h / 0 - 20 °C

2.3: 1 h / 20 °C

3.1: copper(l) iodide / N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere

With copper(l) iodide; tin(IV) chloride; caesium carbonate; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; N,N-dimethyl-formamide; butanone; tert-butyl alcohol;

Reference yield:

: 937-05-3
cis-4-tert-butyl-1-cyclohexanol

: 1621065-12-0
2-(((trans)-4-(tert-butyl)cyclohexyl)oxy)-4-(trifluoromethyl)-1-naphthaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 6 h / Reflux

2.1: tin(IV) chloride / dichloromethane / 2 h / 0 - 20 °C

2.2: 2 h / 0 - 20 °C

2.3: 1 h / 20 °C

3.1: copper(l) iodide / N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere

With copper(l) iodide; di-isopropyl azodicarboxylate; tin(IV) chloride; triphenylphosphine; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; N,N-dimethyl-formamide; toluene;