C₅₈H₆₆O₁₅S₂

Base Information

Chemical Name:C₅₈H₆₆O₁₅S₂
CAS No.:1143516-35-1
Molecular Formula:C₅₈H₆₆O₁₅S₂
Molecular Weight:1067.29
Hs Code.:

C<sub>58</sub>H<sub>66</sub>O<sub>15</sub>S<sub>2</sub>

Synonyms:C₅₈H₆₆O₁₅S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₈H₆₆O₁₅S₂

Chemical Property:

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Technology Process of C₅₈H₆₆O₁₅S₂

There total 14 articles about C₅₈H₆₆O₁₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1143516-30-6
4,6,7-tri-O-benzyl-2,5-O-methylene-D-glycero-D-manno-heptitol-1,3-cyclic sulfate

: 635316-05-1
(2R,3S,4S)-3,4-bis((4-methoxybenzyl)oxy)-2-(((4-methoxybenzyl)oxy)methyl)tetrahydrothiophene

: 1143516-35-1
C₅₈H₆₆O₁₅S₂

Guidance literature:: With potassium carbonate; In 1,1,1,3',3',3'-hexafluoro-propanol; at 75 ℃; for 168h;

Reference yield:

: 28224-73-9
1,3:4,6-di-O-benzylidene-D-mannitol

: 1143516-35-1
C₅₈H₆₆O₁₅S₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydroxide / water

2.1: methanol; toluene-4-sulfonic acid / 2 h / 70 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C

4.2: 0 - 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 h / 20 °C

6.1: sodium hydrogencarbonate; Dess-Martin periodane / 0.25 h / 20 °C

7.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

7.2: -78 - 20 °C

8.1: AD-mix-β / water; tert-butyl alcohol / 168 h / 0 °C

9.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / Cooling with ice bath

9.2: 0 - 20 °C

10.1: methanol; toluene-4-sulfonic acid / 24 h / 20 °C

11.1: thionyl chloride; triethylamine / dichloromethane / 0.75 h / Cooling with ice bath

12.1: sodium periodate / ruthenium trichloride / tetrachloromethane; water; acetonitrile / 2 h / 20 °C

13.1: potassium carbonate / 1,1,1,3',3',3'-hexafluoro-propanol / 168 h / 75 °C / Sealed tube

With 1H-imidazole; methanol; sodium hydroxide; sodium periodate; n-butyllithium; thionyl chloride; AD-mix-β; tetrabutyl ammonium fluoride; sodium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; ruthenium trichloride; In tetrahydrofuran; tetrachloromethane; hexane; dichloromethane; 1,1,1,3',3',3'-hexafluoro-propanol; water; N,N-dimethyl-formamide; acetonitrile; mineral oil; tert-butyl alcohol;

Reference yield:

: 1143516-29-3
4,6,7-tri-O-benzyl-2,5-O-methylene-D-glycero-D-manno-heptitol

: 1143516-35-1
C₅₈H₆₆O₁₅S₂

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride; triethylamine / dichloromethane / 0.75 h / Cooling with ice bath

2: sodium periodate / ruthenium trichloride / tetrachloromethane; water; acetonitrile / 2 h / 20 °C

3: potassium carbonate / 1,1,1,3',3',3'-hexafluoro-propanol / 168 h / 75 °C / Sealed tube

With sodium periodate; thionyl chloride; potassium carbonate; triethylamine; ruthenium trichloride; In tetrachloromethane; dichloromethane; 1,1,1,3',3',3'-hexafluoro-propanol; water; acetonitrile;