N-tert-butyl-3-[(2-amino-5-chloro-4-nitrobenzenecarbonyl)oxy]crotonamide

Base Information

Chemical Name:N-tert-butyl-3-[(2-amino-5-chloro-4-nitrobenzenecarbonyl)oxy]crotonamide
CAS No.:1026651-62-6
Molecular Formula:C₁₅H₁₈ClN₃O₅
Molecular Weight:355.778
Hs Code.:

Synonyms:N-tert-butyl-3-[(2-amino-5-chloro-4-nitrobenzenecarbonyl)oxy]crotonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-tert-butyl-3-[(2-amino-5-chloro-4-nitrobenzenecarbonyl)oxy]crotonamide

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Technology Process of N-tert-butyl-3-[(2-amino-5-chloro-4-nitrobenzenecarbonyl)oxy]crotonamide

There total 2 articles about N-tert-butyl-3-[(2-amino-5-chloro-4-nitrobenzenecarbonyl)oxy]crotonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 34649-02-0
2-amino-5-chloro-4-nitrobenzoic acid

: 10513-45-8
2-tert-butyl-5-methylisoxazolium perchlorate

: 1026651-62-6
N-tert-butyl-3-[(2-amino-5-chloro-4-nitrobenzenecarbonyl)oxy]crotonamide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/S0223-5234(01)01247-8

Reference yield:

: 34649-01-9
2-acetylamino-5-chloro-4-nitrobenzoic acid

: 1026651-62-6
N-tert-butyl-3-[(2-amino-5-chloro-4-nitrobenzenecarbonyl)oxy]crotonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / HOAc; aq. HCl / 1 h / Heating

2: 85 percent / NEt₃ / dimethylformamide / 2 h / 20 °C

With hydrogenchloride; acetic acid; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0223-5234(01)01247-8

Reference yield: 45.0%

: 5696-79-7
(1-naphthylmethyl)guanidine

: 1026651-62-6
N-tert-butyl-3-[(2-amino-5-chloro-4-nitrobenzenecarbonyl)oxy]crotonamide

: N-(2-amino-5-chloro-4-nitro-benzoyl)-N'-naphthalen-1-ylmethyl-guanidine

Guidance literature:: (1-naphthylmethyl)guanidine; With potassium tert-butylate; In 1,4-dioxane; N,N-dimethyl-formamide; at 50 ℃; for 0.166667h;

N-tert-butyl-3-[(2-amino-5-chloro-4-nitrobenzenecarbonyl)oxy]crotonamide; In 1,4-dioxane; N,N-dimethyl-formamide; for 0.333333h; Heating;
DOI:10.1016/S0223-5234(01)01247-8