exo-N-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-2'-deoxycytidine

Base Information

Chemical Name:exo-N-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-2'-deoxycytidine
CAS No.:1016230-31-1
Molecular Formula:C₁₈H₁₇F₄N₇O₅
Molecular Weight:487.37
Hs Code.:

Synonyms:exo-N-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-2'-deoxycytidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of exo-N-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-2'-deoxycytidine

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Technology Process of exo-N-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-2'-deoxycytidine

There total 1 articles about exo-N-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-2'-deoxycytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1016230-41-3
C₃₀H₄₅F₄N₇O₅Si₂

: 1016230-31-1
exo-N-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-2'-deoxycytidine

Guidance literature:: With (HF)n/pyridine; In tetrahydrofuran; at 20 ℃; for 2.5h;
DOI:10.1016/j.tetlet.2007.12.083

Reference yield: 15.0%

: 1016230-31-1
exo-N-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-2'-deoxycytidine

: 5204-74-0
triethylammonium acetate

: exo-N-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-5'-triphosphate-2'-deoxycytidine triethylammonium salt

Guidance literature:: exo-N-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-2'-deoxycytidine; With triethyl phosphate; trichlorophosphate; at 0 ℃; for 4.5h;

With tributyl-amine; tri(n-butyl)ammonium pyrophosphate; In N,N-dimethyl-formamide; at 5 ℃; for 1h;

triethylammonium acetate; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Further stages.;
DOI:10.1016/j.tetlet.2007.12.083