Technology Process of C10H14NO5P
There total 3 articles about C10H14NO5P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
methanol;
at 20 ℃;
for 1h;
DOI:10.1002/cmdc.201000276
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1,1'-carbonyldiimidazole / dichloromethane / 12 h / 20 °C
2.1: trimethylsilyl bromide / dichloromethane / 24 h / 20 °C
2.2: 1 h / 20 °C
3.1: palladium on activated charcoal; hydrogen / methanol / 1 h / 20 °C
With
trimethylsilyl bromide; palladium on activated charcoal; hydrogen; 1,1'-carbonyldiimidazole;
In
methanol; dichloromethane;
DOI:10.1002/cmdc.201000276
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: selenium(IV) oxide; dihydrogen peroxide / tetrahydrofuran; water / 4 h / 65 °C
2.1: 1,1'-carbonyldiimidazole / dichloromethane / 12 h / 20 °C
3.1: trimethylsilyl bromide / dichloromethane / 24 h / 20 °C
3.2: 1 h / 20 °C
4.1: palladium on activated charcoal; hydrogen / methanol / 1 h / 20 °C
With
selenium(IV) oxide; trimethylsilyl bromide; palladium on activated charcoal; hydrogen; dihydrogen peroxide; 1,1'-carbonyldiimidazole;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/cmdc.201000276