((R)-2-Methoxy-1-phenyl-ethyl)-[3-methylsulfanyl-prop-(E)-ylidene]-amine

Base Information

• Chemical Name: ((R)-2-Methoxy-1-phenyl-ethyl)-[3-methylsulfanyl-prop-(E)-ylidene]-amine
• CAS No.: 159116-89-9
• Molecular Formula: C₁₃H₁₉NOS
• Molecular Weight: 237.366

Synonyms:((R)-2-Methoxy-1-phenyl-ethyl)-[3-methylsulfanyl-prop-(E)-ylidene]-amine

Chemical Property of ((R)-2-Methoxy-1-phenyl-ethyl)-[3-methylsulfanyl-prop-(E)-ylidene]-amine

Chemical Property:

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Technology Process of ((R)-2-Methoxy-1-phenyl-ethyl)-[3-methylsulfanyl-prop-(E)-ylidene]-amine

There total 2 articles about ((R)-2-Methoxy-1-phenyl-ethyl)-[3-methylsulfanyl-prop-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3-(methylsulfenyl)propanal (3268-49-3) + (R)-2-methoxy-1-phenylethylamine (64715-85-1,91298-74-7,127180-88-5) → ((R)-2-Methoxy-1-phenyl-ethyl)-[3-methylsulfanyl-prop-(E)-ylidene]-amine (159116-89-9)

Guidance literature:

With sodium sulfate; In benzene; for 1.5h; Ambient temperature;

DOI:10.1021/ja00149a011

Reference yield:

(R)-phenylglycine (875-74-1) → ((R)-2-Methoxy-1-phenyl-ethyl)-[3-methylsulfanyl-prop-(E)-ylidene]-amine (159116-89-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) KH / 1.) THF, overnight, 2.) THF, 3 h

2: 82 percent / Na₂SO₄ / benzene / 1.5 h / Ambient temperature

With potassium hydride; sodium sulfate; In benzene;

DOI:10.1021/ja00149a011

Reference yield: 69.0%

diethyl phosphite lithium salt (72726-66-0) + ((R)-2-Methoxy-1-phenyl-ethyl)-[3-methylsulfanyl-prop-(E)-ylidene]-amine (159116-89-9) → [(R)-1-((R)-2-Methoxy-1-phenyl-ethylamino)-3-methylsulfanyl-propyl]-phosphonic acid diethyl ester (159117-12-1)

Guidance literature:

In tetrahydrofuran; for 20h; Ambient temperature;

DOI:10.1021/ja00099a084

upstream raw materials:

3-(methylsulfenyl)propanal

(R)-2-methoxy-1-phenylethylamine

(R)-phenylglycine

Downstream raw materials:

[(R)-1-((R)-2-Methoxy-1-phenyl-ethylamino)-3-methylsulfanyl-propyl]-phosphonic acid diethyl ester

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