1β-(4-hydroxyphenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

Base Information

• Chemical Name: 1β-(4-hydroxyphenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose
• CAS No.: 1285690-10-9
• Molecular Formula: C₂₉H₅₆O₅Si₃
• Molecular Weight: 569.017

Synonyms:1β-(4-hydroxyphenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

Chemical Property of 1β-(4-hydroxyphenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1β-(4-hydroxyphenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

There total 2 articles about 1β-(4-hydroxyphenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose (1032691-34-1) → 1β-(4-hydroxyphenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose (1285690-10-9)

Guidance literature:

With 2-di-tertbutylphosphino-3,4,5,6-tetramethyl-2',4',6'-triisopropyl-1,1'-biphenyl; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium hydroxide; In 1,4-dioxane; at 55 ℃; for 3h; Inert atmosphere;

DOI:10.1055/s-0030-1258318

Reference yield: 62.0%

1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose (1032691-34-1) → 1β-(4-hydroxyphenyl)-1-deoxy-2,3-di-O-(tert-butyldimethylsilyl)-D-ribofuranose (1285690-15-4) + 1β-(4-hydroxyphenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose (1285690-10-9)

Guidance literature:

With 2-di-tertbutylphosphino-3,4,5,6-tetramethyl-2',4',6'-triisopropyl-1,1'-biphenyl; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium hydroxide; In 1,4-dioxane; at 55 ℃; for 12h; Inert atmosphere;

DOI:10.1055/s-0030-1258318

Reference yield: 77.0%

1β-(4-hydroxyphenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose (1285690-10-9) → 1β-(4-hydroxyphenyl)-1-deoxy-D-ribofuranose (212392-46-6)

Guidance literature:

With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; at 40 ℃; for 48h;

DOI:10.1055/s-0030-1258318

upstream raw materials:

1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

Downstream raw materials:

1β-(4-hydroxyphenyl)-1-deoxy-D-ribofuranose

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1285690-10-9 1β-(4-hydroxyphenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

Send

Send

Metric Ton KG G Pound L ML

Send

Send