1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

Base Information

Chemical Name:1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose
CAS No.:1032691-34-1
Molecular Formula:C₂₉H₅₅BrO₄Si₃
Molecular Weight:631.914
Hs Code.:

Synonyms:1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

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Technology Process of 1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

There total 1 articles about 1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1032691-30-7
1β-(4-bromophenyl)-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

: 1032691-34-1
1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at -10 ℃; for 0.1h; Inert atmosphere;
DOI:10.1002/ejoc.200701168

Reference yield: 95.0%

: 1032691-34-1
1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

: 201230-82-2
carbon monoxide

: 111-92-2
dibutylamine

: 1166385-21-2
1β-[4-(dibutylcarbamoyl)phenyl]-1-deoxy-2,3,5-tri-O-(tert-butyldimethyl-silyl)-D-ribofuranose

Guidance literature:: With potassium phosphate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 80 ℃; for 3h; under 760.051 Torr;
DOI:10.1016/j.tet.2009.04.006

Reference yield: 92.0%

: 110-89-4
piperidine

: 1032691-34-1
1β-(4-bromophenyl)-1-deoxy-2,3,5-tri-O-(tert-butyldimethylsilyl)-D-ribofuranose

: 201230-82-2
carbon monoxide

: 1166385-19-8
1β-{4-[(piperidin-1-yl)carbonyl]phenyl}-1-deoxy-2,3,5-tri-O-(tert-butyldimethyl-silyl)-D-ribofuranose

Guidance literature:: With potassium phosphate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 80 ℃; for 3h; under 760.051 Torr;
DOI:10.1016/j.tet.2009.04.006