tert-butyl N-[{[(tert-butoxy)carbonyl]imino}[(4-hydroxyphenyl)amino]methyl]carbamate

Base Information

• Chemical Name: tert-butyl N-[{[(tert-butoxy)carbonyl]imino}[(4-hydroxyphenyl)amino]methyl]carbamate
• CAS No.: 226087-02-1
• Molecular Formula: C₁₇H₂₅N₃O₅
• Molecular Weight: 351.403

Synonyms:tert-butyl N-[{[(tert-butoxy)carbonyl]imino}[(4-hydroxyphenyl)amino]methyl]carbamate

Chemical Property of tert-butyl N-[{[(tert-butoxy)carbonyl]imino}[(4-hydroxyphenyl)amino]methyl]carbamate

Chemical Property:

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Technology Process of tert-butyl N-[{[(tert-butoxy)carbonyl]imino}[(4-hydroxyphenyl)amino]methyl]carbamate

There total 10 articles about tert-butyl N-[{[(tert-butoxy)carbonyl]imino}[(4-hydroxyphenyl)amino]methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

4-amino-phenol (123-30-8) + N,N'-bis-Boc-S-methyl-isothiourea (322474-21-5) → tert-butyl N-[{[(tert-butoxy)carbonyl]imino}[(4-hydroxyphenyl)amino]methyl]carbamate (226087-02-1)

Guidance literature:

With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 0 ℃; for 3.5h;

DOI:10.1080/00397910008087443

Reference yield: 72.0%

→ tert-butyl N-[{[(tert-butoxy)carbonyl]imino}[(4-hydroxyphenyl)amino]methyl]carbamate (226087-02-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield: 32.0%

4-amino-phenol (123-30-8) + tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate (145013-05-4) → tert-butyl N-[{[(tert-butoxy)carbonyl]imino}[(4-hydroxyphenyl)amino]methyl]carbamate (226087-02-1)

Guidance literature:

With pyridine; mercury dichloride; In N,N-dimethyl-formamide; at 25 ℃; for 48h;

DOI:10.1021/ja9842518

upstream raw materials:

4-amino-phenol

tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate

N,N'-bis-Boc-S-methyl-isothiourea

1,3-di(tert-butyloxycarbonyl)-2-(trifluoromethylsulfonyl)guanidine

Downstream raw materials:

p-N,N'-bis-BOC-guanidinophenyl 2-(2-methoxybenzoyl)benzoate

p-N,N'-bis-BOC-guanidinophenyl 2-(2,5-dimethoxybenzoyl)benzoate

C₂₈H₃₀ClN₃O₈

4-[N',N''-bis(tert-butyloxycarbonyl)guanidino]phenyl N-(benzyloxycarbonyl)-α-(trifluoromethyl)alaninate

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