C₃₄H₄₀N₂O₉S₂Si

Base Information

Chemical Name:C₃₄H₄₀N₂O₉S₂Si
CAS No.:1093121-27-7
Molecular Formula:C₃₄H₄₀N₂O₉S₂Si
Molecular Weight:712.917
Hs Code.:

C<sub>34</sub>H<sub>40</sub>N<sub>2</sub>O<sub>9</sub>S<sub>2</sub>Si

Synonyms:C₃₄H₄₀N₂O₉S₂Si

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Chemical Property of C₃₄H₄₀N₂O₉S₂Si

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Technology Process of C₃₄H₄₀N₂O₉S₂Si

There total 6 articles about C₃₄H₄₀N₂O₉S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 871656-48-3
3-((1S)-2-{[tert-butyl(dimethyl)silyl]oxy}-1-methylethoxy)-5-[4-(methylsulfonyl)phenoxy]-benzoic acid

: 1001327-29-2
4-(2-amino-thiazol-5-yloxy)benzoic acid methyl ester

: 1093121-27-7
C₃₄H₄₀N₂O₉S₂Si

Guidance literature:: 3-((1S)-2-{[tert-butyl(dimethyl)silyl]oxy}-1-methylethoxy)-5-[4-(methylsulfonyl)phenoxy]-benzoic acid; 4-(2-amino-thiazol-5-yloxy)benzoic acid methyl ester; With benzotriazol-1-ol; triethylamine; In dichloromethane; at 20 ℃; for 0.166667h;

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 752242-45-8
3-hydroxy-5-(4-methanesulfonylphenoxy)benzoic acid methyl ester

: 1093121-27-7
C₃₄H₄₀N₂O₉S₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3.75 h / 0 - 20 °C

2.1: lithium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C

2.2: pH 4

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 72 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

5.1: benzotriazol-1-ol; triethylamine / dichloromethane / 0.17 h / 20 °C

5.2: 12 h / 20 °C

With 1H-imidazole; lithium hydroxide; di-isopropyl azodicarboxylate; water; hydrogen; benzotriazol-1-ol; triethylamine; triphenylphosphine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1001419-66-4
C₂₅H₂₆O₇S

: 1093121-27-7
C₃₄H₄₀N₂O₉S₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C

1.2: pH 4

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 72 h / 20 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

4.1: benzotriazol-1-ol; triethylamine / dichloromethane / 0.17 h / 20 °C

4.2: 12 h / 20 °C

With 1H-imidazole; lithium hydroxide; water; hydrogen; benzotriazol-1-ol; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;