tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate

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Chemical Name:tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate
CAS No.:1006689-32-2
Molecular Formula:C₂₅H₃₀N₂O₃
Molecular Weight:406.525
Hs Code.:

Synonyms:tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate

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Chemical Property of tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate

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Technology Process of tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate

There total 1 articles about tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 864682-34-8
3,4-dimethyl-5-[phenyl-(4,4,5-trimethyl-3,4-dihydro-pyrrol-2-ylidene)-methyl]-1H-pyrrole-2-carboxylic acid tert-butyl ester

: 1006689-32-2
tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate

Guidance literature:: With selenium(IV) oxide; In N,N-dimethyl-formamide; at 20 - 80 ℃;
DOI:10.1021/ja0780075

Reference yield: 59.0%

: 1006689-32-2
tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate

: 114037-41-1
5-((5-(tert-butoxycarbonyl)-3,4-dimethyl-1H-pyrrol-2-yl)methyl)-4-(2-(methoxycarbonyl)ethyl)-3-methyl-1H-pyrrole-2-carboxylic acid

: 149-73-5
trimethyl orthoformate

: 2,2,7,8,12,13,18-heptamethyl-5-phenylchlorin-17-propionic acid methyl ester

Guidance literature:: tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate; 5-((5-(tert-butoxycarbonyl)-3,4-dimethyl-1H-pyrrol-2-yl)methyl)-4-(2-(methoxycarbonyl)ethyl)-3-methyl-1H-pyrrole-2-carboxylic acid; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h;

trimethyl orthoformate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 16h; Further stages.;
DOI:10.1021/ja0780075

Reference yield: 38.0%

: 1006689-32-2
tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate

: 88055-49-6
C₂₅H₃₄N₂O₈

: 149-73-5
trimethyl orthoformate

: 17-(methoxycarbonylethyl)-2,2,7,8,12,18-hexamethyl-5-phenyl-chlorin-13-propionic acid methyl ester

Guidance literature:: tert-butyl 5-((14Z)-(5-formyl-3,4-dihydro-4,4-dimethylpyrrol-2-ylidene)-(phenyl)methyl)-3,4-dimethyl-1H-pyrrole-2-carboxylate; C₂₅H₃₄N₂O₈; With trifluoroacetic acid; In dichloromethane; at 20 ℃;

trimethyl orthoformate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; Further stages.;
DOI:10.1021/ja0780075