(S)-N-(3-(benzyloxy)-2-(tert-butyldimethylsilyloxy)propyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

Base Information

Chemical Name:(S)-N-(3-(benzyloxy)-2-(tert-butyldimethylsilyloxy)propyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide
CAS No.:1268368-88-2
Molecular Formula:C₂₆H₃₇NO₄SSi
Molecular Weight:487.736
Hs Code.:

Synonyms:(S)-N-(3-(benzyloxy)-2-(tert-butyldimethylsilyloxy)propyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

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Chemical Property of (S)-N-(3-(benzyloxy)-2-(tert-butyldimethylsilyloxy)propyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

Chemical Property:

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Technology Process of (S)-N-(3-(benzyloxy)-2-(tert-butyldimethylsilyloxy)propyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

There total 3 articles about (S)-N-(3-(benzyloxy)-2-(tert-butyldimethylsilyloxy)propyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₅NO₄SSi

: 106-96-7
propargyl bromide

: 1268368-88-2
(S)-N-(3-(benzyloxy)-2-(tert-butyldimethylsilyloxy)propyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

Guidance literature:: With caesium carbonate; In acetone; toluene; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol200203k

Reference yield:

: 1092363-43-3
(S)-N-(3-(benzyloxy)-2-hydroxypropyl)-4-methylbenzenesulfonamide

: 1268368-88-2
(S)-N-(3-(benzyloxy)-2-(tert-butyldimethylsilyloxy)propyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

2: caesium carbonate / acetone; toluene / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; caesium carbonate; In N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/ol200203k

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1268368-88-2
(S)-N-(3-(benzyloxy)-2-(tert-butyldimethylsilyloxy)propyl)-4-methyl-N-(prop-2-ynyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

2: caesium carbonate / acetone; toluene / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; caesium carbonate; In N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/ol200203k