Technology Process of C45H45BF2N4O8
There total 6 articles about C45H45BF2N4O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C46H49BF2N4O7;
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
With
sodium hydrogencarbonate;
In
dichloromethane; water;
succinic acid anhydride;
With
N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diethylamine / ethanol / 16 h / Reflux
2.1: ammonium acetate / ethanol / 24 h / Reflux
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere
4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16.33 h / 20 °C
5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
5.3: 3 h / 20 °C
With
di-isopropyl azodicarboxylate; ammonium acetate; diethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; dichloromethane;
-
-
1195110-34-9
4,4'-(5,5-difluoro-1,9-diphenyl-5H-4l4,5l4-dipyrrolo[1,2-c:2',1'-f][1,3,5,2]triazaborinine-3,7-diyl)diphenol
- Guidance literature:
-
Multi-step reaction with 3 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 16 h / 20 °C
2: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C
With
di-isopropyl azodicarboxylate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
1: Mitsunobu reaction;
DOI:10.1021/bc100051p