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C45H45BF2N4O8

Base Information
  • Chemical Name:C45H45BF2N4O8
  • CAS No.:1234293-53-8
  • Molecular Formula:C45H45BF2N4O8
  • Molecular Weight:818.682
  • Hs Code.:
C<sub>45</sub>H<sub>45</sub>BF<sub>2</sub>N<sub>4</sub>O<sub>8</sub>

Synonyms:C45H45BF2N4O8

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Chemical Property of C45H45BF2N4O8
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Technology Process of C45H45BF2N4O8

There total 6 articles about C45H45BF2N4O8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
C46H49BF2N4O7; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;
With sodium hydrogencarbonate; In dichloromethane; water;
succinic acid anhydride; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 3h;
Guidance literature:
Multi-step reaction with 5 steps
1.1: diethylamine / ethanol / 16 h / Reflux
2.1: ammonium acetate / ethanol / 24 h / Reflux
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere
4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16.33 h / 20 °C
5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
5.3: 3 h / 20 °C
With di-isopropyl azodicarboxylate; ammonium acetate; diethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane;
Guidance literature:
Multi-step reaction with 3 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 16 h / 20 °C
2: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C
With di-isopropyl azodicarboxylate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; 1: Mitsunobu reaction;
DOI:10.1021/bc100051p
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