1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-cyclohex-1-enyl]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol

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Chemical Name:1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-cyclohex-1-enyl]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol
CAS No.:144396-35-0
Molecular Formula:C₅₇H₇₈O₄Si₂
Molecular Weight:883.415
Hs Code.:

1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-cyclohex-1-enyl]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol

Synonyms:1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-cyclohex-1-enyl]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol

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Chemical Property of 1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-cyclohex-1-enyl]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol

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Technology Process of 1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-cyclohex-1-enyl]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol

There total 5 articles about 1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-cyclohex-1-enyl]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 144396-34-9
C₆₄H₈₄N₂O₆SSi₂

: 144396-35-0
1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-cyclohex-1-enyl]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol

Guidance literature:: With sodium tetrahydroborate; acetic acid;
DOI:10.1016/S0040-4039(00)61222-4

Reference yield:

: 144396-30-5
1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-2-methylene-cyclohex-(E)-ylidene]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol

: 144396-35-0
1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-cyclohex-1-enyl]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / PhNCO / toluene

2: 50 percent / Mo(CO)6, H₂O / acetonitrile

3: 79 percent / CH₃COOH

4: 71 percent / NaBH₄, acetic acid

With sodium tetrahydroborate; hexacarbonyl molybdenum; water; phenyl isocyanate; acetic acid; In toluene; acetonitrile;
DOI:10.1016/S0040-4039(00)61222-4

Reference yield:

: 144396-31-6,144490-20-0
1-((S)-2-{(1R,3aS,7aR)-4-[2-[(8R,10S)-8,10-Bis-(tert-butyl-diphenyl-silanyloxy)-3-methyl-1-oxa-2-aza-spiro[4.5]dec-2-en-(6E)-ylidene]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol

: 144396-35-0
1-((S)-2-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-diphenyl-silanyloxy)-cyclohex-1-enyl]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-propoxy)-2-methyl-propan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / Mo(CO)6, H₂O / acetonitrile

2: 79 percent / CH₃COOH

3: 71 percent / NaBH₄, acetic acid

With sodium tetrahydroborate; hexacarbonyl molybdenum; water; acetic acid; In acetonitrile;
DOI:10.1016/S0040-4039(00)61222-4