Technology Process of C20H21N3O6S
There total 6 articles about C20H21N3O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H25N3O6S;
With
water; lithium hydroxide;
In
tetrahydrofuran;
at 20 ℃;
for 16h;
With
hydrogenchloride;
In
water;
pH=6;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogenchloride; sodium nitrite / ethanol; water / 0.33 h / 0 °C
1.2: 2 h / 0 °C
2.1: ammonium acetate; acetic acid / 0.75 h / 120 °C / Microwave irradiation
3.1: sulfur; morpholine / ethanol / 0.42 h / 130 °C / Microwave irradiation
4.1: dmap; di-tert-butyl dicarbonate / 4 h / 20 °C
5.1: caesium carbonate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C
6.1: water; lithium hydroxide / tetrahydrofuran / 16 h / 20 °C
6.2: pH 6
With
morpholine; hydrogenchloride; dmap; di-tert-butyl dicarbonate; ammonium acetate; water; caesium carbonate; sulfur; acetic acid; lithium hydroxide; sodium nitrite;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ammonium acetate; acetic acid / 0.75 h / 120 °C / Microwave irradiation
2.1: sulfur; morpholine / ethanol / 0.42 h / 130 °C / Microwave irradiation
3.1: dmap; di-tert-butyl dicarbonate / 4 h / 20 °C
4.1: caesium carbonate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C
5.1: water; lithium hydroxide / tetrahydrofuran / 16 h / 20 °C
5.2: pH 6
With
morpholine; dmap; di-tert-butyl dicarbonate; ammonium acetate; water; caesium carbonate; sulfur; acetic acid; lithium hydroxide;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
