1,3-bis((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazolium bromide

Base Information

• Chemical Name: 1,3-bis((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazolium bromide
• CAS No.: 1374403-65-2
• Molecular Formula: Br*C₅₁H₅₂BrN₂O₆
• Molecular Weight: 948.792

Synonyms:1,3-bis((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazolium bromide

Chemical Property of 1,3-bis((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazolium bromide

Chemical Property:

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Technology Process of 1,3-bis((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazolium bromide

There total 4 articles about 1,3-bis((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-7-bis(bromomethyl)naphthalene (1374403-63-0) + 1-((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazole (1374403-64-1) → 1,3-bis((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazolium bromide (1374403-65-2)

Guidance literature:

In acetonitrile; at 60 ℃; for 48h;

DOI:10.1002/anie.201108404

Reference yield:

2,7-bis(bromomethyl)naphthalene (38309-89-6) → 1,3-bis((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazolium bromide (1374403-65-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 0.17 h / 20 °C

1.2: 20 °C

2.1: acetonitrile / 48 h / 60 °C

With potassium carbonate; In acetonitrile;

DOI:10.1002/anie.201108404

Reference yield:

4-[2-(allyloxy)ethoxy]phenol (111915-32-3) → 1,3-bis((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazolium bromide (1374403-65-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 0.17 h / 20 °C

1.2: 20 °C

2.1: acetonitrile / 48 h / 60 °C

With potassium carbonate; In acetonitrile;

DOI:10.1002/anie.201108404

upstream raw materials:

4-[2-(allyloxy)ethoxy]phenol

2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-7-bis(bromomethyl)naphthalene

1-((2-((4-(2-(allyloxy)ethoxy)phenoxy)methyl)-naphthalen-7-yl)methyl)-2-bromo-4,5-dimethyl-1H-imidazole

2,7-bis(bromomethyl)naphthalene

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