1-(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy-6-O-acetyl-7-deacetyl-forskolin

Base Information

Chemical Name:1-(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy-6-O-acetyl-7-deacetyl-forskolin
CAS No.:1350722-11-0
Molecular Formula:C₃₂H₄₃N₃O₇
Molecular Weight:581.709
Hs Code.:

Synonyms:1-(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy-6-O-acetyl-7-deacetyl-forskolin

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Chemical Property of 1-(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy-6-O-acetyl-7-deacetyl-forskolin

Chemical Property:

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Technology Process of 1-(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy-6-O-acetyl-7-deacetyl-forskolin

There total 3 articles about 1-(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy-6-O-acetyl-7-deacetyl-forskolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350721-66-2
1-O-propargyl-6-O-acetyl-7-deacetyl-forskolin

: 622-79-7
benzyl azide

: 1350722-11-0
1-(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy-6-O-acetyl-7-deacetyl-forskolin

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; for 1h; regioselective reaction;
DOI:10.1016/j.tetlet.2011.08.154

Reference yield:

: 100-39-0
benzyl bromide

: 1350722-11-0
1-(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy-6-O-acetyl-7-deacetyl-forskolin

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / water; dimethyl sulfoxide

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 1 h

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.154

Reference yield:

: 66575-29-9,64657-11-0
forskolin

: 1350722-11-0
1-(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy-6-O-acetyl-7-deacetyl-forskolin

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetone / 24 h / Reflux

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 1 h

With copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; potassium iodide; In water; acetone; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.154