tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxo-1-(tetrahydro-2H-pyran-4-ylmethyl)ethyl}benzoate

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Chemical Name:tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxo-1-(tetrahydro-2H-pyran-4-ylmethyl)ethyl}benzoate
CAS No.:1080060-08-7
Molecular Formula:C₂₁H₃₁NO₅
Molecular Weight:377.481
Hs Code.:

Synonyms:tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxo-1-(tetrahydro-2H-pyran-4-ylmethyl)ethyl}benzoate

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Chemical Property of tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxo-1-(tetrahydro-2H-pyran-4-ylmethyl)ethyl}benzoate

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Technology Process of tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxo-1-(tetrahydro-2H-pyran-4-ylmethyl)ethyl}benzoate

There total 1 articles about tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxo-1-(tetrahydro-2H-pyran-4-ylmethyl)ethyl}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 101691-94-5
4-(iodomethyl)tetrahydro-2H-pyran

: 1080060-07-6
tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxoethyl}benzoate

: 12125-02-9
ammonium chloride

: 1080060-08-7
tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxo-1-(tetrahydro-2H-pyran-4-ylmethyl)ethyl}benzoate

Guidance literature:: tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxoethyl}benzoate; ammonium chloride; With lithium diisopropyl amide; In tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; at -78 ℃; for 1h;

4-(iodomethyl)tetrahydro-2H-pyran; In tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; at -78 ℃; for 3h;

With water; ammonium chloride; In tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone;

Reference yield: 91.0%

: 1080060-08-7
tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxo-1-(tetrahydro-2H-pyran-4-ylmethyl)ethyl}benzoate

: 1826-67-1
vinyl magnesium bromide

: 1080060-09-8
tert-butyl 4-[2-oxo-1-(tetrahydro-2H-pyran-4-ylmethyl)but-3-en-1-yl]benzoate

Guidance literature:: tert-butyl 4-{2-[methoxy(methyl)amino]-2-oxo-1-(tetrahydro-2H-pyran-4-ylmethyl)ethyl}benzoate; vinyl magnesium bromide; In tetrahydrofuran; at -78 - 20 ℃;

With hydrogenchloride; water; In tetrahydrofuran;