2-(5-(4-(2-morpholinoethoxy)phenyl)pyridin-2-yl)-N-benzylacetamide mesylate

Base Information

• Chemical Name: 2-(5-(4-(2-morpholinoethoxy)phenyl)pyridin-2-yl)-N-benzylacetamide mesylate
• CAS No.: 1080645-95-9
• Molecular Formula: CH₄O₃S*C₂₆H₂₉N₃O₃
• Molecular Weight: 527.642

Synonyms:2-(5-(4-(2-morpholinoethoxy)phenyl)pyridin-2-yl)-N-benzylacetamide mesylate

Chemical Property of 2-(5-(4-(2-morpholinoethoxy)phenyl)pyridin-2-yl)-N-benzylacetamide mesylate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

KX2-391mesylate >98% ^*data from reagent suppliers

Safty Information:

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Technology Process of 2-(5-(4-(2-morpholinoethoxy)phenyl)pyridin-2-yl)-N-benzylacetamide mesylate

There total 6 articles about 2-(5-(4-(2-morpholinoethoxy)phenyl)pyridin-2-yl)-N-benzylacetamide mesylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

KX2-391 (897016-82-9) + methanesulfonic acid (75-75-2,98527-29-8) → 2-(5-(4-(2-morpholinoethoxy)phenyl)pyridin-2-yl)-N-benzylacetamide mesylate (1080645-95-9)

Guidance literature:

In acetone; at 27 - 50 ℃; for 28.6167h;

Reference yield:

N-(2-chlorethyl)morpholine (3240-94-6) → 2-(5-(4-(2-morpholinoethoxy)phenyl)pyridin-2-yl)-N-benzylacetamide mesylate (1080645-95-9)

Guidance literature:

Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water

3: sodium hexamethyldisilazane / Cooling with ice

4: sulfuric acid

5: methoxybenzene / Heating

6: acetone / 50 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; sodium hexamethyldisilazane; sodium carbonate; potassium carbonate; methoxybenzene; In 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; acetone; 1: |Williamson Ether Synthesis / 2: |Suzuki Coupling;

Reference yield:

4-bromo-phenol (106-41-2) → 2-(5-(4-(2-morpholinoethoxy)phenyl)pyridin-2-yl)-N-benzylacetamide mesylate (1080645-95-9)

Guidance literature:

Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water

3: sodium hexamethyldisilazane / Cooling with ice

4: sulfuric acid

5: methoxybenzene / Heating

6: acetone / 50 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; sodium hexamethyldisilazane; sodium carbonate; potassium carbonate; methoxybenzene; In 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; acetone; 1: |Williamson Ether Synthesis / 2: |Suzuki Coupling;

upstream raw materials:

KX2-391

methanesulfonic acid

N-(2-chlorethyl)morpholine

4-bromo-phenol

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