4-azido-3-methylbenzoyl hydrazide

Base Information

Chemical Name:4-azido-3-methylbenzoyl hydrazide
CAS No.:380922-32-7
Molecular Formula:C₈H₉N₅O
Molecular Weight:191.192
Hs Code.:

Synonyms:4-azido-3-methylbenzoyl hydrazide

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Chemical Property of 4-azido-3-methylbenzoyl hydrazide

Chemical Property:

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Technology Process of 4-azido-3-methylbenzoyl hydrazide

There total 3 articles about 4-azido-3-methylbenzoyl hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N'-(4-azido-3-methyl-benzoyl)-hydrazinecarboxylic acid tert-butyl ester

: 380922-32-7
4-azido-3-methylbenzoyl hydrazide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/jm010231w

Reference yield:

: 845866-42-4
methyl 4-azido-3-methylbenzoate

: 380922-32-7
4-azido-3-methylbenzoyl hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 25percent aq. NaOH / ethanol / 1 h / 20 °C

2: EDCI; 4-(N,N-dimethylamino)pyridine / tetrahydrofuran; dimethylformamide / 17 h / 20 °C

3: 1.02 g / trifluoroacetic acid / CH₂Cl₂ / 2 h / 0 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm010231w

Reference yield:

: 380922-31-6
4-azido-3-methylbenzoic acid

: 380922-32-7
4-azido-3-methylbenzoyl hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: EDCI; 4-(N,N-dimethylamino)pyridine / tetrahydrofuran; dimethylformamide / 17 h / 20 °C

2: 1.02 g / trifluoroacetic acid / CH₂Cl₂ / 2 h / 0 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm010231w