Technology Process of C13H7F4N3
There total 3 articles about C13H7F4N3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
copper(l) iodide; cis-N,N'-dimethyl-1,2-diaminocyclohexane;
In
N,N-dimethyl-formamide;
at 140 ℃;
for 1.5h;
microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 144 h
2.1: acetic anhydride; potassium acetate; acetic acid; isopentyl nitrite / toluene / 1 h / Reflux
2.2: 1 h / Reflux
3.1: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / N,N-dimethyl-formamide / 1.5 h / 140 °C / microwave irradiation
With
potassium acetate; acetic anhydride; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; isopentyl nitrite;
dmap; copper(l) iodide; cis-N,N'-dimethyl-1,2-diaminocyclohexane;
In
dichloromethane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: acetic anhydride; potassium acetate; acetic acid; isopentyl nitrite / toluene / 1 h / Reflux
1.2: 1 h / Reflux
2.1: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / N,N-dimethyl-formamide / 1.5 h / 140 °C / microwave irradiation
With
potassium acetate; acetic anhydride; potassium carbonate; acetic acid; isopentyl nitrite;
copper(l) iodide; cis-N,N'-dimethyl-1,2-diaminocyclohexane;
In
N,N-dimethyl-formamide; toluene;