Technology Process of C30H31FO9S2
There total 12 articles about C30H31FO9S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
urea hydrogen peroxide adduct;
In
methanol; acetonitrile;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: lithium chloride; isopropylmagnesium chloride / tetrahydrofuran / 1 h / Cooling with ice
1.2: 1 h
2.1: cerium(III) chloride heptahydrate / methanol / 0.33 h / 20 °C
2.2: 1 h / -78 °C
3.1: acetic acid / water / 15 h / 100 °C
3.2: 2 h / 20 °C / Cooling with ice
4.1: hydrogen bromide; acetic acid / 1 h / 20 °C / Cooling with ice
5.1: thiourea / acetonitrile / 1 h / Reflux
6.1: triethylamine / 1 h / 20 °C
7.1: urea hydrogen peroxide adduct / acetonitrile; methanol / 20 °C
With
cerium(III) chloride heptahydrate; hydrogen bromide; isopropylmagnesium chloride; urea hydrogen peroxide adduct; acetic acid; triethylamine; thiourea; lithium chloride;
In
tetrahydrofuran; methanol; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: cerium(III) chloride heptahydrate / methanol / 0.33 h / 20 °C
1.2: 1 h / -78 °C
2.1: acetic acid / water / 15 h / 100 °C
2.2: 2 h / 20 °C / Cooling with ice
3.1: hydrogen bromide; acetic acid / 1 h / 20 °C / Cooling with ice
4.1: thiourea / acetonitrile / 1 h / Reflux
5.1: triethylamine / 1 h / 20 °C
6.1: urea hydrogen peroxide adduct / acetonitrile; methanol / 20 °C
With
cerium(III) chloride heptahydrate; hydrogen bromide; urea hydrogen peroxide adduct; acetic acid; triethylamine; thiourea;
In
methanol; water; acetonitrile;
