1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylthio)-2-thiouracil

Base Information

Chemical Name:1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylthio)-2-thiouracil
CAS No.:125057-24-1
Molecular Formula:C₁₉H₂₈N₂O₃S₂Si
Molecular Weight:424.66
Hs Code.:

Synonyms:1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylthio)-2-thiouracil

Suppliers and Price of 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylthio)-2-thiouracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylthio)-2-thiouracil

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Technology Process of 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylthio)-2-thiouracil

There total 2 articles about 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylthio)-2-thiouracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116457-79-5
1-(2-acetoxyethoxy methyl)-2-thiouracil

: 125057-24-1
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylthio)-2-thiouracil

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 1 N NaOH / ethanol / 0.17 h / Ambient temperature

2: 69 percent / imidazole / dimethylformamide / 14 h / Ambient temperature

3: 1.) LDA / 1.) THF, -70 deg C, 1 h, 2.) -70 deg C, 15 min

With 1H-imidazole; sodium hydroxide; lithium diisopropyl amide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00108a023

Reference yield:

: 125057-23-0
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-2-thiouracil

: 882-33-7
diphenyldisulfane

: 125057-24-1
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylthio)-2-thiouracil

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -70 deg C, 1 h, 2.) -70 deg C, 15 min;
DOI:10.1021/jm00108a023