Technology Process of C14H16F5NO5S
There total 4 articles about C14H16F5NO5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
acetonitrile;
at 20 ℃;
for 1.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / toluene / 2 h / Inert atmosphere; Reflux
1.2: pH 9
2.1: 1-butyl-3-methylimidazolium Tetrafluoroborate; 2,6-di-tert-butyl-pyridine / 16 h / 150 °C
3.1: hydrogen / 5%-palladium/activated carbon / water; methanol / 48 h / 20 °C
4.1: hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 1.5 h / 20 °C
With
hydrogenchloride; 2,6-di-tert-butyl-pyridine; hydrogen; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-butyl-3-methylimidazolium Tetrafluoroborate;
5%-palladium/activated carbon;
In
methanol; water; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-butyl-3-methylimidazolium Tetrafluoroborate; 2,6-di-tert-butyl-pyridine / 16 h / 150 °C
2: hydrogen / 5%-palladium/activated carbon / water; methanol / 48 h / 20 °C
3: hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 1.5 h / 20 °C
With
hydrogenchloride; 2,6-di-tert-butyl-pyridine; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-butyl-3-methylimidazolium Tetrafluoroborate;
5%-palladium/activated carbon;
In
methanol; water; acetonitrile;
